You are performing an aqueous extraction, and you forget which layer is the organic layer and which is the aqueous layer. What is the best way to solve this problem? a. Add a small amount of sodium sulfate - if it dissolves, the layer is water. b. Remove all the solvents via rotary evaporation and start again. c. Pick the top layer, as this is always the organic layer. d. Smell the two layers to see which one is an organic solvent.

Chemistry
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Author:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
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Chapter1: Chemical Foundations
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You are performing an aqueous extraction, and you forget which layer is the organic layer and which is the aqueous layer. What is the best way to solve this problem?

a. Add a small amount of sodium sulfate - if it dissolves, the layer is water.

b. Remove all the solvents via rotary evaporation and start again.

c. Pick the top layer, as this is always the organic layer.

d. Smell the two layers to see which one is an organic solvent.

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