Write out a detailed recipe for the preparation of benzalacetophenone.

Organic Chemistry
9th Edition
ISBN:9781305080485
Author:John E. McMurry
Publisher:John E. McMurry
Chapter21: Carboxylic Acid Derivatives: Nucleophilic Acyl Substitution Reactions
Section21.SE: Something Extra
Problem 54AP: The following reactivity order has been found for the saponification of alkyl acetates by aqueous...
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Background: In an experiment, dibenzalacetone is prepared using a Claisen-Schmidt reaction between aceton and two equivalents of benzaldehyde. [Image 1]

Write out a detailed recipe for the preparation of benzalacetophenone. [Image 2]

Write out a detailed recipe for the preparation of benzalacetophenone.
Transcribed Image Text:Write out a detailed recipe for the preparation of benzalacetophenone.
In this experiment, we will prepare dibenzalacetone using a Claisen-Schmidt reaction (an exam-
ple of a crossed aldol condensation) between acetone and two equivalents of benzaldehyde:
CHS
NaOH
-C-H + CH3-
+ 2 H20
CH=CH-C-CH=CH-
Transcribed Image Text:In this experiment, we will prepare dibenzalacetone using a Claisen-Schmidt reaction (an exam- ple of a crossed aldol condensation) between acetone and two equivalents of benzaldehyde: CHS NaOH -C-H + CH3- + 2 H20 CH=CH-C-CH=CH-
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