Which of the following correlations about the analyses of iodine and saponification numbers is/are incorrect? a. Alcoholic KOH: dissolve KOH to lipid sample b. Hanus reagent: react with saturated lipid bond c. Reflux set-up: hasten reaction d. Blank titration: determine total mol of KOH 2. A triacylglycerol (Sample X) was subjected to saponification analysis. 1.1 grams of the sample was refluxed with 5% alcoholic KOH and the refluxed solution was titrated with 17.2 mL of 0.44 M HCl titrant. The blank solution was titrated with 25.6 mL of the titrant. i. What is the saponification number of the sample? ii. Which of the following could be the identity of the sample? Show solutions pls a. Tripalmitin (MW: 807.3) b. Trilaurin (MW: 639.8) c. Triolein (MW: 885:4) d. Tristearin (MW: 891.48)
1.Which of the following correlations about the analyses of iodine and saponification
numbers is/are incorrect?
a. Alcoholic KOH: dissolve KOH to lipid sample
b. Hanus reagent: react with saturated lipid bond
c. Reflux set-up: hasten reaction
d. Blank titration: determine total mol of KOH
2. A triacylglycerol (Sample X) was subjected to saponification analysis. 1.1 grams of the
sample was refluxed with 5% alcoholic KOH and the refluxed solution was titrated with 17.2 mL
of 0.44 M HCl titrant. The blank solution was titrated with 25.6 mL of the titrant.
i. What is the saponification number of the sample?
ii. Which of the following could be the identity of the sample? Show solutions pls
a. Tripalmitin (MW: 807.3)
b. Trilaurin (MW: 639.8)
c. Triolein (MW: 885:4)
d. Tristearin (MW: 891.48)
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