Chemistry
10th Edition
ISBN:9781305957404
Author:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Publisher:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Chapter1: Chemical Foundations
Section: Chapter Questions
Problem 1RQ: Define and explain the differences between the following terms. a. law and theory b. theory and...
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Question
What is the limiting reagent and theoretical yield?
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S
Corrine Costello
Arpose: The purpose of this expertiment is to make oynthette luciferin (elivanilly! ouclate)
by treating venillin us oxalyl chloricle
SimUText Summer
2020
Experimental Aeparabon i Chemiluminescence of Divenillyl Osalate
S
HO
EtŐ Ac
OCH3
OCH3
Skype
Reageat Table
Chamisal
71-
Kulalall MP(OcBPOC)mmol mcos (a) elemaitylylom volune Iml)
0320
$4.dmg
Vanillin
152.95
81-83
NA
2.1
I,48
Ielyl Chlaridı 126,93
Intethelamine Lol. 19.
609
6.31
NA
61
2.05
.1332
0.326
0902
NA
NA
9.28
2.23
0.22606
AIA
5.2.
16
3646
B0% hychegun 34.61447
NIA
15
0.5469
AIA
NIA
AIA
nIA
peroxicle
1OMNOH
Tricabin
Pendere
1.
40.0
218.21
252.316
358.364
14
25%
276-279 NA
0.04
3.48
0.006
NIA
15.9
G-024
208-211
0.525 2
NIA
Oralate
MA
5.25
1.88
ed
9:17 AM
9:16 AM
| at 8:47 PM
at 8:47 PM
at 8:37 PM
| at 8:37 PM
at 12:14 PM
| at 11:47 AM
| at 11:33 AM
021 at 11:12 PM
021 at 11:11 PM
021 at 8:49 PM
021 at 5:46 PM
Signature
Date
Witness/TA
Date
021 at 5:44 PM
021 at 4:57 PM
THE HAYDEN-MCNEIL STUDENT LAB NOTEBOOK
Note: Insert Divider Under Copy Sheet Before Writing
021 at 3:28 PM
021 at 3:18 PM
021 at 8:43 PM
121 at 8:40 PM.
APR
15
AATO04
W](/v2/_next/image?url=https%3A%2F%2Fcontent.bartleby.com%2Fqna-images%2Fquestion%2F648a503f-5830-49a4-82fc-a3290c26979f%2F70346191-0bd0-4211-bcbb-4fea01aabab8%2F5gdi6yj_processed.png&w=3840&q=75)
Transcribed Image Text:Preview
File
Edit
View
Go
Window Help
Tools
10% (4)
Thu 9:18 AM
a orgo pic
Search
S
Corrine Costello
Arpose: The purpose of this expertiment is to make oynthette luciferin (elivanilly! ouclate)
by treating venillin us oxalyl chloricle
SimUText Summer
2020
Experimental Aeparabon i Chemiluminescence of Divenillyl Osalate
S
HO
EtŐ Ac
OCH3
OCH3
Skype
Reageat Table
Chamisal
71-
Kulalall MP(OcBPOC)mmol mcos (a) elemaitylylom volune Iml)
0320
$4.dmg
Vanillin
152.95
81-83
NA
2.1
I,48
Ielyl Chlaridı 126,93
Intethelamine Lol. 19.
609
6.31
NA
61
2.05
.1332
0.326
0902
NA
NA
9.28
2.23
0.22606
AIA
5.2.
16
3646
B0% hychegun 34.61447
NIA
15
0.5469
AIA
NIA
AIA
nIA
peroxicle
1OMNOH
Tricabin
Pendere
1.
40.0
218.21
252.316
358.364
14
25%
276-279 NA
0.04
3.48
0.006
NIA
15.9
G-024
208-211
0.525 2
NIA
Oralate
MA
5.25
1.88
ed
9:17 AM
9:16 AM
| at 8:47 PM
at 8:47 PM
at 8:37 PM
| at 8:37 PM
at 12:14 PM
| at 11:47 AM
| at 11:33 AM
021 at 11:12 PM
021 at 11:11 PM
021 at 8:49 PM
021 at 5:46 PM
Signature
Date
Witness/TA
Date
021 at 5:44 PM
021 at 4:57 PM
THE HAYDEN-MCNEIL STUDENT LAB NOTEBOOK
Note: Insert Divider Under Copy Sheet Before Writing
021 at 3:28 PM
021 at 3:18 PM
021 at 8:43 PM
121 at 8:40 PM.
APR
15
AATO04
W
![Name:
Prelab: Preparation and Chemiluminescence of Divanillyl Oxalate
Reaction equation:
Reagent Table
mass (g) density volume
(g/mL)
Chemical
FW
mp (°C) bp (°C)
mmol
(g/mol)
(mL)
vanillin
N/A
N/A
NA
oxalyl chloride
triethylamine
ethyl acetate
|1.0 М HСI
N/A
NA
NA
NA
N/A
N/A
30% hydrogen peroxide
NA
N/A
N/A
1.0 M NaOH
NA
N/A
N/A
triacetin
NA
perylene
divanillyl oxalate
Note: For those reagents that are in solution, the FW, mmol, and mass columns refer to the solute in
N/A
N/A
N/A
N/A
N/A
N/A
the solution.
Limiting reagent:
Theoretical yield:](/v2/_next/image?url=https%3A%2F%2Fcontent.bartleby.com%2Fqna-images%2Fquestion%2F648a503f-5830-49a4-82fc-a3290c26979f%2F70346191-0bd0-4211-bcbb-4fea01aabab8%2Fiafilyh_processed.png&w=3840&q=75)
Transcribed Image Text:Name:
Prelab: Preparation and Chemiluminescence of Divanillyl Oxalate
Reaction equation:
Reagent Table
mass (g) density volume
(g/mL)
Chemical
FW
mp (°C) bp (°C)
mmol
(g/mol)
(mL)
vanillin
N/A
N/A
NA
oxalyl chloride
triethylamine
ethyl acetate
|1.0 М HСI
N/A
NA
NA
NA
N/A
N/A
30% hydrogen peroxide
NA
N/A
N/A
1.0 M NaOH
NA
N/A
N/A
triacetin
NA
perylene
divanillyl oxalate
Note: For those reagents that are in solution, the FW, mmol, and mass columns refer to the solute in
N/A
N/A
N/A
N/A
N/A
N/A
the solution.
Limiting reagent:
Theoretical yield:
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