Chemistry
10th Edition
ISBN:9781305957404
Author:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Publisher:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Chapter1: Chemical Foundations
Section: Chapter Questions
Problem 1RQ: Define and explain the differences between the following terms. a. law and theory b. theory and...
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What is the limiting reagent and theoretical yield?
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Corrine Costello
Arpose: The purpose of this expertiment is to make oynthette luciferin (elivanilly! ouclate)
by treating venillin us oxalyl chloricle
SimUText Summer
2020
Experimental Aeparabon i Chemiluminescence of Divenillyl Osalate
S
HO
EtŐ Ac
OCH3
OCH3
Skype
Reageat Table
Chamisal
71-
Kulalall MP(OcBPOC)mmol mcos (a) elemaitylylom volune Iml)
0320
$4.dmg
Vanillin
152.95
81-83
NA
2.1
I,48
Ielyl Chlaridı 126,93
Intethelamine Lol. 19.
609
6.31
NA
61
2.05
.1332
0.326
0902
NA
NA
9.28
2.23
0.22606
AIA
5.2.
16
3646
B0% hychegun 34.61447
NIA
15
0.5469
AIA
NIA
AIA
nIA
peroxicle
1OMNOH
Tricabin
Pendere
1.
40.0
218.21
252.316
358.364
14
25%
276-279 NA
0.04
3.48
0.006
NIA
15.9
G-024
208-211
0.525 2
NIA
Oralate
MA
5.25
1.88
ed
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APR
15
AATO04
W
Transcribed Image Text:Name:
Prelab: Preparation and Chemiluminescence of Divanillyl Oxalate
Reaction equation:
Reagent Table
mass (g) density volume
(g/mL)
Chemical
FW
mp (°C) bp (°C)
mmol
(g/mol)
(mL)
vanillin
N/A
N/A
NA
oxalyl chloride
triethylamine
ethyl acetate
|1.0 М HСI
N/A
NA
NA
NA
N/A
N/A
30% hydrogen peroxide
NA
N/A
N/A
1.0 M NaOH
NA
N/A
N/A
triacetin
NA
perylene
divanillyl oxalate
Note: For those reagents that are in solution, the FW, mmol, and mass columns refer to the solute in
N/A
N/A
N/A
N/A
N/A
N/A
the solution.
Limiting reagent:
Theoretical yield:
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