Homework Help is Here – Start Your Trial Now!
Science
Chemistry
Upon completing a reaction in the lab, you determine the percent yield for the process to be 140%. Obviously, something isn't right. You double check your math and everything is good from that end. You take a melting point, which is close to the literature value. You take an IR and notice an extra strong signal at 1700 cm-1 that doesn't match what you would expect on your compound. You don't notice a broad signal above 3000 cm1. Of the possibilities, which would be the most probably given your elevated yield? The sample wasn't sufficiently dried and has water in it. You recall that you washed the sample with acetone. You must not have evaporated all of the acetone away. O Your sample has an impurity from the reaction. O You only weighed out 90% of your isolated compound.

Upon completing a reaction in the lab, you determine the percent yield for the process to be 140%. Obviously, something isn't right. You double check your math and everything is good from that end. You take a melting point, which is close to the literature value. You take an IR and notice an extra strong signal at 1700 cm-1 that doesn't match what you would expect on your compound. You don't notice a broad signal above 3000 cm1. Of the possibilities, which would be the most probably given your elevated yield? The sample wasn't sufficiently dried and has water in it. You recall that you washed the sample with acetone. You must not have evaporated all of the acetone away. O Your sample has an impurity from the reaction. O You only weighed out 90% of your isolated compound.

Chemistry
Chemistry
10th Edition
ISBN:9781305957404
Author:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Publisher:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Chapter1: Chemical Foundations
Section: Chapter Questions
Problem 1RQ: Define and explain the differences between the following terms. a. law and theory b. theory and...
See similar textbooks
icon
Related questions
Question
Upon completing a reaction in the lab, you determine the percent yield for the process to be 140%. Obviously, something isn't right. You double check your math and everything is good from that end. You take a melting point, which is close to the literature value. You take an IR and notice an extra strong signal at 1700 cm 1 that doesn't match what you would expect on your compound. You don't notice a broad signal above 3000 cm-1. Of the possibilities, which would be the most probably given your elevated yield? O The sample wasn't sufficiently dried and has water in it. You recall that you washed the sample with acetone. You must not have evaporated all of the acetone away. Your sample has an impurity from the reaction. You only weighed out 90% of your isolated compound.
Transcribed Image Text:Upon completing a reaction in the lab, you determine the percent yield for the process to be 140%. Obviously, something isn't right. You double check your math and everything is good from that end. You take a melting point, which is close to the literature value. You take an IR and notice an extra strong signal at 1700 cm 1 that doesn't match what you would expect on your compound. You don't notice a broad signal above 3000 cm-1. Of the possibilities, which would be the most probably given your elevated yield? O The sample wasn't sufficiently dried and has water in it. You recall that you washed the sample with acetone. You must not have evaporated all of the acetone away. Your sample has an impurity from the reaction. You only weighed out 90% of your isolated compound.
Expert Solution
trending now

Trending now

This is a popular solution!

steps

Step by step

Solved in 2 steps with 2 images

SEE SOLUTIONCheck out a sample Q&A here
Blurred answer
Knowledge Booster
Spectroanalytical Methods
Learn more about
Need a deep-dive on the concept behind this application? Look no further. Learn more about this topic, chemistry and related others by exploring similar questions and additional content below.
Similar questions
  • SEE MORE QUESTIONS
Recommended textbooks for you
Chemistry
Chemistry
Chemistry
ISBN:
9781305957404
Author:
Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Publisher:
Cengage Learning
Chemistry
Chemistry
Chemistry
ISBN:
9781259911156
Author:
Raymond Chang Dr., Jason Overby Professor
Publisher:
McGraw-Hill Education
Principles of Instrumental Analysis
Principles of Instrumental Analysis
Chemistry
ISBN:
9781305577213
Author:
Douglas A. Skoog, F. James Holler, Stanley R. Crouch
Publisher:
Cengage Learning
Organic Chemistry
Organic Chemistry
Chemistry
ISBN:
9780078021558
Author:
Janice Gorzynski Smith Dr.
Publisher:
McGraw-Hill Education
Chemistry: Principles and Reactions
Chemistry: Principles and Reactions
Chemistry
ISBN:
9781305079373
Author:
William L. Masterton, Cecile N. Hurley
Publisher:
Cengage Learning
Elementary Principles of Chemical Processes, Bind…
Elementary Principles of Chemical Processes, Bind…
Chemistry
ISBN:
9781118431221
Author:
Richard M. Felder, Ronald W. Rousseau, Lisa G. Bullard
Publisher:
WILEY
SEE MORE TEXTBOOKS