TRANCESE Relative Intensity Unknown #5 Elemental Analysis: 69.72% Carbon, 11.70% Hydrogen, 18.57% Oxygen Mass Spec 100 --1501 80- 60 40 20- to 10 20 30 40 50 60 70 IR m/z 4000 3000 2000 1500 1000 500 1H NMR 13C NMR 11 10 ppm Exchanges 200 190 150 120 200 Chemical Formula: HDI Calculation: Proposed Structure: with D₂O
TRANCESE Relative Intensity Unknown #5 Elemental Analysis: 69.72% Carbon, 11.70% Hydrogen, 18.57% Oxygen Mass Spec 100 --1501 80- 60 40 20- to 10 20 30 40 50 60 70 IR m/z 4000 3000 2000 1500 1000 500 1H NMR 13C NMR 11 10 ppm Exchanges 200 190 150 120 200 Chemical Formula: HDI Calculation: Proposed Structure: with D₂O
Principles of Instrumental Analysis
7th Edition
ISBN:9781305577213
Author:Douglas A. Skoog, F. James Holler, Stanley R. Crouch
Publisher:Douglas A. Skoog, F. James Holler, Stanley R. Crouch
Chapter19: Nuclear Magnetic Resonance Spectroscopy
Section: Chapter Questions
Problem 19.33QAP
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Transcribed Image Text:TRANCESE
Relative Intensity
Unknown #5
Elemental Analysis:
69.72% Carbon, 11.70% Hydrogen, 18.57% Oxygen
Mass Spec
100
--1501
80-
60
40
20-
to
10
20
30
40
50
60
70
IR
m/z
4000
3000
2000 1500
1000
500
1H NMR
13C NMR
11
10
ppm
Exchanges
200 190 150
120 200
Chemical Formula:
HDI Calculation:
Proposed Structure:
with
D₂O
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