The literature melting point of 1-phenylcyclohexanol is 59-62 °C. The melting point range you observed d) for your recovered 1-phenylcyclohexanol is 50-55 °C. Is your 1-phenylcyclohexanol pure or impure? How do you know? Please be specific.

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**Discussion on Melting Point Analysis**

**Question:**

d) The literature melting point of 1-phenylcyclohexanol is 59-62 °C. The melting point range you observed for your recovered 1-phenylcyclohexanol is 50-55 °C. Is your 1-phenylcyclohexanol pure or impure? How do you know? Please be specific.

---

**Explanation:**

In this context, we're analyzing the purity of a sample of 1-phenylcyclohexanol based on its melting point. 

1. **Literature Melting Point:** 59-62 °C - This range is considered the standard or expected melting point for pure 1-phenylcyclohexanol.

2. **Observed Melting Point:** 50-55 °C - This is the melting point range measured for the recovered sample.

**Analysis:**

- **Comparison:** The observed melting point range of 50-55 °C is lower than the literature value of 59-62 °C.
  
- **Implication of Lower Melting Point:** A lower melting point, along with a broader melting range, usually indicates the presence of impurities. Pure substances typically have a sharp melting point that corresponds closely to the literature value. 

Therefore, based on the lower and broader observed melting point range, it can be concluded that the recovered 1-phenylcyclohexanol sample is likely impure. The presence of impurities disrupts the orderly lattice structure of the solid, causing it to melt at a lower temperature.
Transcribed Image Text:**Discussion on Melting Point Analysis** **Question:** d) The literature melting point of 1-phenylcyclohexanol is 59-62 °C. The melting point range you observed for your recovered 1-phenylcyclohexanol is 50-55 °C. Is your 1-phenylcyclohexanol pure or impure? How do you know? Please be specific. --- **Explanation:** In this context, we're analyzing the purity of a sample of 1-phenylcyclohexanol based on its melting point. 1. **Literature Melting Point:** 59-62 °C - This range is considered the standard or expected melting point for pure 1-phenylcyclohexanol. 2. **Observed Melting Point:** 50-55 °C - This is the melting point range measured for the recovered sample. **Analysis:** - **Comparison:** The observed melting point range of 50-55 °C is lower than the literature value of 59-62 °C. - **Implication of Lower Melting Point:** A lower melting point, along with a broader melting range, usually indicates the presence of impurities. Pure substances typically have a sharp melting point that corresponds closely to the literature value. Therefore, based on the lower and broader observed melting point range, it can be concluded that the recovered 1-phenylcyclohexanol sample is likely impure. The presence of impurities disrupts the orderly lattice structure of the solid, causing it to melt at a lower temperature.
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