Standard Addition Variable Volume Calibration Curve i. Use the following data and Excel to plot a standard addition variable volume calibration curve. Use your curve to determine the concentration (ppm) of the unknown sample. Save your calibration curve as a PDF file and upload to eClass. Use the following additional information to complete the table below. total volume (volume of standard + sample) volume of standard added . V ii. iii. Vs • Vo initial volume of sample= 50.0 mL S₁ initial concentration of standard = 279 ppm Is+x= signal measured for a sample containing unknown plus standard
Standard Addition Variable Volume Calibration Curve i. Use the following data and Excel to plot a standard addition variable volume calibration curve. Use your curve to determine the concentration (ppm) of the unknown sample. Save your calibration curve as a PDF file and upload to eClass. Use the following additional information to complete the table below. total volume (volume of standard + sample) volume of standard added . V ii. iii. Vs • Vo initial volume of sample= 50.0 mL S₁ initial concentration of standard = 279 ppm Is+x= signal measured for a sample containing unknown plus standard
Chemistry
10th Edition
ISBN:9781305957404
Author:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Publisher:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Chapter1: Chemical Foundations
Section: Chapter Questions
Problem 1RQ: Define and explain the differences between the following terms. a. law and theory b. theory and...
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Transcribed Image Text:c) Standard Addition Variable Volume Calibration Curve
i.
ii.
iii.
Vs (ml)
0.0
0.05
0.25
0.40
0.55
0.70
0.85
1.0
1.15
Use the following data and Excel to plot a standard addition variable volume
calibration curve. Use your curve to determine the concentration (ppm) of the
unknown sample.
Save your calibration curve as a PDF file and upload to eClass.
Use the following additional information to complete the table below.
• V = total volume (volume of standard + sample)
• Vs = volume of standard added
• Vo initial volume of sample = 50.0 mL
• S₁ = initial concentration of standard = 279 ppm
• Is+x = signal measured for a sample containing unknown plus standard
V total (mL)
50.0
50.05
50.25
50.4
?
?
?
?
?
x-variable
Si *Vs/V. (ppm)
0.0
0.279
1.395
2.232
?
?
?
?
?
I(s+x) (μA)
1.84
1.95
2.81
3.5
3.88
4.39
4.86
5.45
5.67
y-variable
I(s+x) *V/V. (μA)
1.84
1.95195
2.82405
3.528
?
?
?
?
?
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