Sam knows that he has one of 3 possible liquid unknowns: tetrahyrofuran (bp 65-67°C), ethyl acetate (bp 76-77°C), or toluene (bp 110-111°C). He sets up for a microscale bp determination and clamps the whole shebang in a water bath. Fifteen minutes late the water is boiling like crazy, but he has yet to see a single vapor bubble escape from the capillary tube. He double-checks his set-up and everything is fine so now he’s totally confused. What must his unknown be and why? Break it to him gently…he doesn’t want to feel like a total idiot.

Chemistry
10th Edition
ISBN:9781305957404
Author:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Publisher:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Chapter1: Chemical Foundations
Section: Chapter Questions
Problem 1RQ: Define and explain the differences between the following terms. a. law and theory b. theory and...
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Sam knows that he has one of 3 possible liquid unknowns: tetrahyrofuran (bp 65-67°C), ethyl acetate
(bp 76-77°C), or toluene (bp 110-111°C). He sets up for a microscale bp determination and clamps the
whole shebang in a water bath. Fifteen minutes late the water is boiling like crazy, but he has yet to
see a single vapor bubble escape from the capillary tube. He double-checks his set-up and everything
is fine so now he’s totally confused. What must his unknown be and why? Break it to him gently…he
doesn’t want to feel like a total idiot.

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