QUESTIONS 1) How will the following affect the TLC separation? a) too much sample applied. b) Stationary phase is too active. c) Forgetting to remove the plate when the solvent has reached the top of the plate. d) Having too much solvent in the developing chamber so that its surface extends above the origin. e) Polarity of the solvent being too high. 2) Which dye would be more soluble in n-propyl alcohol, the blue or the yellow? How can you tell? 3) Which compound is more strongly adsorbed on silica, ortho- or para- nitroaniline? Correlate the R, values with the structures.

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Author:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
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QUESTIONS
D. How will the following affect the TLC separation?
a) too much sample applied.
b) Stationary phase is too active.
c) Forgetting to remove the plate when the solvent has reached the
of the plate.
top
d) Having too much solvent in the developing chamber so that its
surface extends above the origin.
e) Polarity of the solvent being too high.
2) Which dye would be more soluble in n-propyl alcohol, the blue or the
yellow? How can you tell?
3) Which compound is more strongly adsorbed on silica, ortho- or para-
nitroaniline? Correlate the R, values with the structures.
76
Transcribed Image Text:QUESTIONS D. How will the following affect the TLC separation? a) too much sample applied. b) Stationary phase is too active. c) Forgetting to remove the plate when the solvent has reached the of the plate. top d) Having too much solvent in the developing chamber so that its surface extends above the origin. e) Polarity of the solvent being too high. 2) Which dye would be more soluble in n-propyl alcohol, the blue or the yellow? How can you tell? 3) Which compound is more strongly adsorbed on silica, ortho- or para- nitroaniline? Correlate the R, values with the structures. 76
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