NMR (500 MHz) 7.75 7.70 7.65 7.60 -7.63 -7.60 -7.50 -7.48 7.55 7.50 7.45 7.40 7.35 -7.18 -6500000 -6000000 -5500000 -5000000 4500000 -4000000 -3500000 -3000000 -2500000 -2000000 -1500000 -1000000 -500000 -500000 7.30 7.25 7.20 f1 (ppm) 7.15 7.10 7.05 7.00 6.95 6.90 6.85 6.80 NMR (500 MHz) -1.59 -6500000 -6000000 -5500000 5000000 -4500000 -4000000 -3500000 -3000000 -2500000 -2000000 -1500000 -1000000 -500000 ידיידי 861 T 2.99 3.00- 500000 8.0 7.5 7.0 6.5 6.0 5.5 5.0 4.5 4.0 3.5 3.0 2.5 2.0 1.5 1.0 0.5 0.0 f1 (ppm)

NMR (500 MHz) 7.75 7.70 7.65 7.60 -7.63 -7.60 -7.50 -7.48 7.55 7.50 7.45 7.40 7.35 -7.18 -6500000 -6000000 -5500000 -5000000 4500000 -4000000 -3500000 -3000000 -2500000 -2000000 -1500000 -1000000 -500000 -500000 7.30 7.25 7.20 f1 (ppm) 7.15 7.10 7.05 7.00 6.95 6.90 6.85 6.80 NMR (500 MHz) -1.59 -6500000 -6000000 -5500000 5000000 -4500000 -4000000 -3500000 -3000000 -2500000 -2000000 -1500000 -1000000 -500000 ידיידי 861 T 2.99 3.00- 500000 8.0 7.5 7.0 6.5 6.0 5.5 5.0 4.5 4.0 3.5 3.0 2.5 2.0 1.5 1.0 0.5 0.0 f1 (ppm)

Principles of Instrumental Analysis

7th Edition

ISBN:9781305577213

Author:Douglas A. Skoog, F. James Holler, Stanley R. Crouch

Publisher:Douglas A. Skoog, F. James Holler, Stanley R. Crouch

Chapter34: Particle Size Determination

Section: Chapter Questions

Problem 34.9QAP

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COMPOUND 1 INFRARED SPECTRUM 4800 3000 2000 1500 s000 MRVEMUSERI 1906 77 1598 S0 1819 1492 20 1366 1166 77 108? 21 B16 38 798 21 712 50 707 S4 SA7 B4 3270 21 56 1358 53 1345 50 1299 1238 9259 21 COMPOUND 1 2955 74 1029 2939 68 17 66 2924 2054 2727 4. 1454 1408 1378 1209 838 26 42 53 1176 24 10 656 67 49 833 25 620 50
Wavenumbers (cm-¹) 4000 3000 2000 1500 1000 500 D 1511 1236 3423 1033 3348 827 transmittance [%] 3074 3052 3042 2839 1631 1971 1862 1888 1740 001
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