Draw A to G structure. (МеO),CHCSA, CH,Cl2(1) 1 equiv. NaHTHF, 0 °CDIBAH, -78 °CHO.30 minBA0°C, 10 minrt, 24 h(2)Br1 st gen. Grubbs cat.H2, Pd/CD (C16H2806)ECH2CI2, 40 °C, 2hELOH, rt, 12 h(1) 2 equiv. NaHTHF, 0 °C6 M HCIG (C12H2604)THErt,1 h(2) 1 equiv.BrBrCyclization

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(МеO);CH CSA, CH,Cl2 DIBAH, -78 °C 30 min (1) 1 equiv. NaH THF, 0 °C HO, A rt, 24 h 0°C, 10 min Br (2) 1 st gen. Grubbs cat. H2, Pd/C D (C16H2806) E CH,Cl2, 40 °C, 2 h ELOH, rt, 12 h (1) 2 equiv. NaH THF, 0 °C 6 M HCI F G (C12H2604) THE rt,1 h (2) 1 equiv. Br Br Cyclization

(МеO);CH CSA, CH,Cl2 DIBAH, -78 °C 30 min (1) 1 equiv. NaH THF, 0 °C HO, A rt, 24 h 0°C, 10 min Br (2) 1 st gen. Grubbs cat. H2, Pd/C D (C16H2806) E CH,Cl2, 40 °C, 2 h ELOH, rt, 12 h (1) 2 equiv. NaH THF, 0 °C 6 M HCI F G (C12H2604) THE rt,1 h (2) 1 equiv. Br Br Cyclization

Chemistry for Engineering Students

4th Edition

ISBN:9781337398909

Author:Lawrence S. Brown, Tom Holme

Publisher:Lawrence S. Brown, Tom Holme

Chapter10: Entropy And The Second Law Of Thermodynamics

Section: Chapter Questions

Problem 10.72PAE

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Concept explainers

Solutions

Solutions can be considered as homogeneous mixtures which contain two or more than two chemical substances. The chemical substance which is the greater part is defined as solvent. And the chemical substance that is dissolved in a solvent is referred to as solute. Solution chemistry plays an important role in chemistry since it supports many commercial applications of solutions.

Question

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Draw A to G structure.

(МеO),CH
CSA, CH,Cl2
(1) 1 equiv. NaH
THF, 0 °C
DIBAH, -78 °C
HO.
30 min
B
A
0°C, 10 min
rt, 24 h
(2)
Br
1 st gen. Grubbs cat.
H2, Pd/C
D (C16H2806)
E
CH2CI2, 40 °C, 2h
ELOH, rt, 12 h
(1) 2 equiv. NaH
THF, 0 °C
6 M HCI
G (C12H2604)
THE
rt,1 h
(2) 1 equiv.
Br
Br
Cyclization

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