i) You did the following reaction, worked up in Ethyl Acetate and Water. ၀ Did your reaction work? What are the extra peaks in the NMR spectrum? 10 Chem Shift 1.27 2.03 2.35 3.65 4.15 4.61 5.28 7.11 7.25 9.54 NaBH₂ CH₂Cl₂ solvent Integral 0.036 0.035 1.53 0.50 0.023 1.03 0.005 1.01 1.05 0.003 OH Multiplicity triplet singlet singlet singlet (removed by D20 shake) quartet singlet PPM singlet doublet doublet singlet

Chemistry
10th Edition
ISBN:9781305957404
Author:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Publisher:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Chapter1: Chemical Foundations
Section: Chapter Questions
Problem 1RQ: Define and explain the differences between the following terms. a. law and theory b. theory and...
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i) You did the following reaction, worked up in Ethyl Acetate and Water.
NaBH
6=6
CH₂Cl₂ solvent
Did your reaction work? What are the extra peaks in the NMR spectrum?
10
Chem Shift
1.27
2.03
2.35
3.65
4.15
4.61
5.28
7.11
7.25
9.54
Integral
0.036
0.035
1.53
0.50
OH
0.023
1.03
0.005
1.01
1.05
0.003
Multiplicity
triplet
singlet
singlet
singlet (removed by D20 shake)
quartet
singlet
singlet
doublet
PPM
doublet
singlet
Transcribed Image Text:i) You did the following reaction, worked up in Ethyl Acetate and Water. NaBH 6=6 CH₂Cl₂ solvent Did your reaction work? What are the extra peaks in the NMR spectrum? 10 Chem Shift 1.27 2.03 2.35 3.65 4.15 4.61 5.28 7.11 7.25 9.54 Integral 0.036 0.035 1.53 0.50 OH 0.023 1.03 0.005 1.01 1.05 0.003 Multiplicity triplet singlet singlet singlet (removed by D20 shake) quartet singlet singlet doublet PPM doublet singlet
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