How would you interpret this IR spectroscopy of 9-fluorenone? Some background information is that this was a lab to separate fluorene and 9-fluorenone. It should be noted that other solids and solvents used during the column chromatography was alumina, sand, petroleum ether, and dichloromethane. The original compound was 0.05 g but it yielded 0.03 g 9-fluorenone. There may or may not be impurities. %T100-105-% T100-9590-8580-400040003000300020002000Lab Solutions LabSolutions IR¥Data CHEM23 Spring 2023*MW Dhimitruka*AR and GJ -'ellow.ispd2315001712.79-1597.06-1448.54-1500ItemSample nameSample IDOptionIntensity Mode1456910 ResolutionApodizationNo. of Scans1000AR and GJ - Yellow916.19-734.88-516.921000164 cm-1405.05500Valuemaycm-1366.48500% TransmittanceHapp-Genzel360.69cm-1Peak123Intensity1 360.69 87.34366.48 89.44405.05 97.33516.92 99.75734.88 99.03916.19 99.571448.54 99.531597.06 99.481712.79 99.334567819Corr.Intensity11.809.352.040.210.570.250.120.130.31Base (H) Base (L)Area362.62 356.83 38.7161372.26 362.62 48.605412.77 401.19 19.015518.85 513.07 0.759740.67 711.73 18.761923.90 904.61 6.4601458.18 1444.68 5.1561602.85 1587.42 7.1601724.36 1693.50 16.223SHIMADZUCorr.Area43.69244.3004.8530.5608.7432.9860.7281.0844.632Comment

IR spectra deals results from the interaction of infrared radiation with matter by absorption. IR…

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Chemistry

10th Edition

ISBN:9781305957404

Author:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste

Publisher:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste

Chapter1: Chemical Foundations

Section: Chapter Questions

Problem 1RQ: Define and explain the differences between the following terms. a. law and theory b. theory and...

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How would you interpret this IR spectroscopy of 9-fluorenone? Some background information is that this was a lab to separate fluorene and 9-fluorenone. It should be noted that other solids and solvents used during the column chromatography was alumina, sand, petroleum ether, and dichloromethane. The original compound was 0.05 g but it yielded 0.03 g 9-fluorenone. There may or may not be impurities.

%T
100-
105-
% T
100-
95
90-
85
80-
4000
4000
3000
3000
2000
2000
Lab Solutions LabSolutions IR¥Data CHEM
23 Spring 2023*MW Dhimitruka*AR and GJ -
'ellow.ispd
2
3
1500
1712.79-
1597.06-
1448.54-
1500
Item
Sample name
Sample ID
Option
Intensity Mode
14
5
6
9
10 Resolution
Apodization
No. of Scans
1000
AR and GJ - Yellow
916.19-
734.88-
516.92
1000
16
4 cm-1
405.05
500
Value
may
cm-1
366.48
500
% Transmittance
Happ-Genzel
360.69
cm-1
Peak
12
3
Intensity
1 360.69 87.34
366.48 89.44
405.05 97.33
516.92 99.75
734.88 99.03
916.19 99.57
1448.54 99.53
1597.06 99.48
1712.79 99.33
4
5
6
7
8
19
Corr.
Intensity
11.80
9.35
2.04
0.21
0.57
0.25
0.12
0.13
0.31
Base (H) Base (L)
Area
362.62 356.83 38.716
1372.26 362.62 48.605
412.77 401.19 19.015
518.85 513.07 0.759
740.67 711.73 18.761
923.90 904.61 6.460
1458.18 1444.68 5.156
1602.85 1587.42 7.160
1724.36 1693.50 16.223
SHIMADZU
Corr.
Area
43.692
44.300
4.853
0.560
8.743
2.986
0.728
1.084
4.632
Comment

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