How can we know that the NMR for cyclohexanone is in fact cyclohexanone( the NMR for cyclohexanone is not labeled). Analyze the spectra to prove
How can we know that the NMR for cyclohexanone is in fact cyclohexanone( the NMR for cyclohexanone is not labeled). Analyze the spectra to prove
Chemistry
10th Edition
ISBN:9781305957404
Author:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Publisher:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Chapter1: Chemical Foundations
Section: Chapter Questions
Problem 1RQ: Define and explain the differences between the following terms. a. law and theory b. theory and...
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An oxidation reaction was conducted using cyclohexanol and NaOCl to make cyclohexanone. How can we know that the NMR for cyclohexanone is in fact cyclohexanone( the NMR for cyclohexanone is not labeled). Analyze the spectra to prove its identity along with the NMR of the starting material which is the spectra labeled cyclohexanol below.
Transcribed Image Text:471
BRUKER
I222
|TV ||
Current Data Paramet ers
Feb20-2020-chem22:
67
NAME
EXPNO
PROCNO
1
Cyclohexanol in CDC13
F2 - Acquisition Parameter
Date
Time
20200220
23.13
INSTRUM
PROBHD
spect
5 mm PABBO вв-
zg30
32768
PULPROG
TD
SOLVENT
NS
CDC13
2
DS
SWH
5208.333 Hz
0.158946 Hz
3.1457281 sec
16
96.000 usec
25.61 usec
298.0 K
FIDRES
AQ
RG
DW
DE
ТЕ
D1
1.50000000 sec
TDO
1
------- CHANNEL f1
NUC1
P1
-- -
-
1H
11.38 usec
-2.50 dB
18.35869598 w
PL1
PL1W
SFO1
400.1320007 MH2
F2 - Processing parameters
SI
SF
32768
400.1300065 MHz
WDW
SSB
EM
0.30 Hz
LB
GB
PC
1.00
7.5
7.0
6.5
6.0
5.5
5.0
4.5
4.0
3.5
3.0
2.5
2.0
1.5
1.0
ppm
888
Transcribed Image Text:3
...
BRUKER
Current Data Paramet ers
NAME
EXPNO
Feb18-2020-chem22:
3
PROCNO
1
F2 - Acquisition Paramet er
Date_
Time
INSTRUM
PROBHD
20200218
17.31
spect
5 mm PABBO BB-
zg30
32768
CDC13
2
1.8 1.7
1.6 ppm
PULPROG
TD
SOLVENT
2.9
2.8
2.7
2.6
2.5
2.4 2.3
2.2
2.1
2.0
1.9
NS
DS
SWH
5208.333 Hz
0.158946 Hz
3.1457281 sec
64
96.000 usec
FIDRES
AQ
RG
DW
DE
25.61 usec
298.0 K
1.50000000 sec
1
TE
D1
TDO
CHANNEL f1 =--
1H
11.38 usec
-2.50 dB
18.35869598 W
400.1320007 MH2
===== =-
NUC1
P1
PL1
PL1W
SFO1
F2 - Processing parameterS
32768
400.1300065 MHz
SI
SF
WDW
EM
SB
LB
0.30 Hz
GB
PC
1.00
11
10
8
7
6
5
4
3
2
1
ppm
000'
2.32
1.044
-2.08
88:I
98:T/
1.85
1.70
1.70
69'I
89
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