Homework Help is Here – Start Your Trial Now!
Science
Chemistry
From the attached procedures, make a table consisting of all the compounds and their respective molecular weight (g/mol), density (g/ml), volume (ml), weight (g), mole and ratio. Take caution to ensure that the molecular weight is the CORRECT literature value.

From the attached procedures, make a table consisting of all the compounds and their respective molecular weight (g/mol), density (g/ml), volume (ml), weight (g), mole and ratio. Take caution to ensure that the molecular weight is the CORRECT literature value.

Chemistry
Chemistry
10th Edition
ISBN:9781305957404
Author:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Publisher:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Chapter1: Chemical Foundations
Section: Chapter Questions
Problem 1RQ: Define and explain the differences between the following terms. a. law and theory b. theory and...
See similar textbooks
icon
Related questions
Question
100%

From the attached procedures, make a table consisting of all the compounds and their respective molecular weight (g/mol), density (g/ml), volume (ml), weight (g), mole and ratio. Take caution to ensure that the molecular weight is the CORRECT literature value. 

Procedure: Synthesis of a Cyalume™M CI OH CI Ar- CI O Procedure: Chemiluminescence 0. CI Ar TM Synthesis and Analysis of a Cyalume ™M H₂O₂ base 2 CI OH Place 0.8 g of 2,4,6-trichlorophenol and 10 mL of toluene into a 50 mL round bottom flask and stir to dissolve. Add 0.56 mL of triethylamine (caution - stinks!!!) and cool the solution in an ice bath. Add 0.2 mL of oxalyl chloride (caution - lachrymator!) dropwise over 30 seconds via syringe. Attach a condenser to the flask, then heat the reaction mixture to 75 degrees in a water bath for 30 minutes. A solid will form. Cool the reaction to room temperature, then add 10 mL hexanes. Place the reaction flask on ice and stir for 5 minutes. Filter the solid, then rinse the solid with more hexanes. Place the solid in a 50 mL Erlenmeyer flask and add 10 mL of water. Break up the large chunks with a stir rod and shake the flask to dissolve all triethylamine salt byproducts. Filter the solid and rinse with water. Press dry, then recrystallize your ester from ethyl acetate or toluene. CI NET3 toluene 0 °C -> 75 °C CI O-O 0 CI 1,2-dioxetanedione CI 2 CI CO₂* 0 0 oc fluorescer CI fluorescer* CI CO₂ fluorescer + hv In a 10 dram vial, dissolve 100 mg of your ester in 20 mL of diethyl phthalate. Add a drop of one fluorophore solution and 100 mg of sodium salicylate. Add cap and shake to mix. To your ester suspension, add 2 mL of the peroxide suspension (3mL 30% hydrogen peroxide diluted to 100 mL with diethyl phthalate). Replace the cap and shake to mix.
Transcribed Image Text:Procedure: Synthesis of a Cyalume™M CI OH CI Ar- CI O Procedure: Chemiluminescence 0. CI Ar TM Synthesis and Analysis of a Cyalume ™M H₂O₂ base 2 CI OH Place 0.8 g of 2,4,6-trichlorophenol and 10 mL of toluene into a 50 mL round bottom flask and stir to dissolve. Add 0.56 mL of triethylamine (caution - stinks!!!) and cool the solution in an ice bath. Add 0.2 mL of oxalyl chloride (caution - lachrymator!) dropwise over 30 seconds via syringe. Attach a condenser to the flask, then heat the reaction mixture to 75 degrees in a water bath for 30 minutes. A solid will form. Cool the reaction to room temperature, then add 10 mL hexanes. Place the reaction flask on ice and stir for 5 minutes. Filter the solid, then rinse the solid with more hexanes. Place the solid in a 50 mL Erlenmeyer flask and add 10 mL of water. Break up the large chunks with a stir rod and shake the flask to dissolve all triethylamine salt byproducts. Filter the solid and rinse with water. Press dry, then recrystallize your ester from ethyl acetate or toluene. CI NET3 toluene 0 °C -> 75 °C CI O-O 0 CI 1,2-dioxetanedione CI 2 CI CO₂* 0 0 oc fluorescer CI fluorescer* CI CO₂ fluorescer + hv In a 10 dram vial, dissolve 100 mg of your ester in 20 mL of diethyl phthalate. Add a drop of one fluorophore solution and 100 mg of sodium salicylate. Add cap and shake to mix. To your ester suspension, add 2 mL of the peroxide suspension (3mL 30% hydrogen peroxide diluted to 100 mL with diethyl phthalate). Replace the cap and shake to mix.
Expert Solution
trending now

Trending now

This is a popular solution!

steps

Step by step

Solved in 3 steps

SEE SOLUTIONCheck out a sample Q&A here
Blurred answer
Knowledge Booster
Iodine Titrations
Learn more about
Need a deep-dive on the concept behind this application? Look no further. Learn more about this topic, chemistry and related others by exploring similar questions and additional content below.
Similar questions
  • SEE MORE QUESTIONS
Recommended textbooks for you
Chemistry
Chemistry
Chemistry
ISBN:
9781305957404
Author:
Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Publisher:
Cengage Learning
Chemistry
Chemistry
Chemistry
ISBN:
9781259911156
Author:
Raymond Chang Dr., Jason Overby Professor
Publisher:
McGraw-Hill Education
Principles of Instrumental Analysis
Principles of Instrumental Analysis
Chemistry
ISBN:
9781305577213
Author:
Douglas A. Skoog, F. James Holler, Stanley R. Crouch
Publisher:
Cengage Learning
Organic Chemistry
Organic Chemistry
Chemistry
ISBN:
9780078021558
Author:
Janice Gorzynski Smith Dr.
Publisher:
McGraw-Hill Education
Chemistry: Principles and Reactions
Chemistry: Principles and Reactions
Chemistry
ISBN:
9781305079373
Author:
William L. Masterton, Cecile N. Hurley
Publisher:
Cengage Learning
Elementary Principles of Chemical Processes, Bind…
Elementary Principles of Chemical Processes, Bind…
Chemistry
ISBN:
9781118431221
Author:
Richard M. Felder, Ronald W. Rousseau, Lisa G. Bullard
Publisher:
WILEY
SEE MORE TEXTBOOKS