draw the curly arrow mechanism for this experiment, include all details like electrons, curly arrows, by products etc 3. Formation of trichloroacetimidate donor2,2,3,3'4',6,6'-Hepta-O-acetyl-B-D-lactose trichloroacetimidate (3)OACACOLOAcCl3CCNAcoLOACK₂CO3AcODCMOACACO-OAcNHCompoundMW (g/mol) eqn (mmol)d (g/ml)Sugar (crude)636.5514.71Trichloroacetonitrile144.398.51.44Potassium carbonate138.213DCM84.931.33Apparatus: 50 round bottom flask, N₂ atmosphereReaction temperature: RTReaction time:TLC: EtOAc/Tol 1:1 + 1% NET,Reaction molarity: 0.2 MThe crude sugar is dissolved in dry DCM, trichloroacetonitrile and potassium carbonate are added.Stirring at RT until starting material is consumed. After complete conversion, the solution is filtered,concentrated in vacuo (water bath not warmer than 30 °C). Crude is used directly for next reaction.C26H36018636.5532OHAcOOACACO-m (g)LOACOACC28H36C13NO 18780.9403V (ml)CCI

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Answered: draw the curly arrow mechanism for this…

Science

Chemistry

draw the curly arrow mechanism for this experiment, include all details like electrons, curly arrows, by products etc

Organic Chemistry

9th Edition

ISBN:9781305080485

Author:John E. McMurry

Publisher:John E. McMurry

Chapter25: Biomolecules: Carbohydrates

Section25.SE: Something Extra

Problem 69AP

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