Based on the given chromatograph, answer the following questions: 1) Which of the diet sodas have the highest concentration of caffeine? Which standard best reflects this concentration? 2) Which of the diet sodas have the lowest concentration of aspartame? Which standard best reflects this concentration? 3) What is the approximate retention time of benzoate?

Based on the given chromatograph, answer the following questions: 1) Which of the diet sodas have the highest concentration of caffeine? Which standard best reflects this concentration? 2) Which of the diet sodas have the lowest concentration of aspartame? Which standard best reflects this concentration? 3) What is the approximate retention time of benzoate?

Chemistry

10th Edition

ISBN:9781305957404

Author:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste

Publisher:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste

Chapter1: Chemical Foundations

Section: Chapter Questions

Problem 1RQ: Define and explain the differences between the following terms. a. law and theory b. theory and...

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A scientist wishes to measure the concentration of methyl benzoate in a plant stream by gas chromatography. He prepares a sample of butyl benzoate to use as an internal standard. The results of a preliminary run, which used a solution known to contain 1.35 mg/mL of methyl B benzoate (peak A) and 1.49 mg/mL of butyl benzoate (peak B), are shown. The area of peak A is determined to be 319 and the area of peak B is determined to be 381 measured in arbitrary units by the computer. To measure the sample, 1.00 mL of a standard sample of butyl benzoate containing 2.27 mg/mL is mixed with 1.00 mL of the plant stream material. Analysis of the mixture gave a peak area of 10 Time (min) 15 465 for peak A and 397 for pcak B. What is the concentration of methyl benzoate in the plant stream? methyl benzoate concentration: mg/mL Detector Response
Below is the procedure described for determination of paracetamol according to BP: "Weigh and powder 20 tablets. Add a quantity of powder equivalent to about 0.35 g paracetamol to 50 ml of 0.1 M NaOH, dilute with water to 200 ml and shake for 15 min. Add sufficient water to make up 250 ml. Filter the solution and dilute 5 ml of the filtrate to 100 ml with water. Dilute further 10 ml to 100 ml. Measure the absorbance at 257 nm. The A, = 715 at 257 nm". Which of the following is correct? O a. An analyst can take 0.37g of the powdered tablets instead of 0.35. O b. An analyst can replace NaOH with HCl O c. An analyst can skip the shaking step O d. B andC O e. All of the above
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A scientist wishes to measure the concentration of methyl benzoate in a plant stream by gas chromatography. He prepares a sample of butyl benzoate to use as an internal standard. The results of a preliminary run, which used a solution known to contain 1.37 mg/mL of methyl benzoate (peak A) and 1.51 mg/mL of butyl benzoate (peak B), are shown. The area of peak A is determined to be 3.40×102 and the area of peak B is determined to be 398 measured in arbitrary units by the computer. To measure the sample, 1.00 mL of a standard sample of butyl benzoate containing 2.49 mg/mL is mixed with 1.00 mL of the plant stream material. Analysis of the mixture gave a peak area of 437 for peak A and 415 for peak B. What is the concentration of methyl benzoate in the plant stream?
Question 28
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7
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