B. Metathesis to [Ru(phen)3)]Cl2 The dry [Ru(phen)3] [PF6]2 from Step A is placed in a 250 mL beaker and dissolved in 50 to 100 mL dry acetone (add enough to be completely dissolved), if any solids observed filter through medium porosity glass frit. Transfer the filtrate to a 250 mL beaker and start gently stirring with a stir bar. Separately, dissolve 1.25 g Bu4NCI in 25 mL dry acetone. Add the Bu4NCI solution to the [Ru(phen)3]2+ solution dropwise until it appears that further additions do not induce further precipitation. Filter product with a 60 mL medium porosity glass frit. Wash with 20 mL acetone and dry in oven at 60-80C. Record yield.

B. Metathesis to [Ru(phen)3)]Cl2 The dry [Ru(phen)3] [PF6]2 from Step A is placed in a 250 mL beaker and dissolved in 50 to 100 mL dry acetone (add enough to be completely dissolved), if any solids observed filter through medium porosity glass frit. Transfer the filtrate to a 250 mL beaker and start gently stirring with a stir bar. Separately, dissolve 1.25 g Bu4NCI in 25 mL dry acetone. Add the Bu4NCI solution to the [Ru(phen)3]2+ solution dropwise until it appears that further additions do not induce further precipitation. Filter product with a 60 mL medium porosity glass frit. Wash with 20 mL acetone and dry in oven at 60-80C. Record yield.

Chemistry

10th Edition

ISBN:9781305957404

Author:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste

Publisher:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste

Chapter1: Chemical Foundations

Section: Chapter Questions

Problem 1RQ: Define and explain the differences between the following terms. a. law and theory b. theory and...

See similar textbooks

Similar questions

29 minutes, 42 seconds. Question Completion Status: A Moving to another question will save this response. Question 15 What is not an expected product of the following allylic substitution reaction? NBS, hv Br Br Compounds II and II Compound II only O Compound I only O Compound II only A Moving to another question will save this response O O C
Please help me solve this synthesis. Show all steps of the mechanism. Thank you!
Please answer in tipping format
In each reaction box, place the best reagent and conditions from the list. 1) CEN 2) 3) 4) 5) Answer Bank NANH, NaBH, acetone CH,CH, MgBr (excess) acetic acid acetate ion CH,OH, H,O* (cat.) LIAIH, (CH,),CHMgBr (excess) CH,MgBr (excess) H,0 H,0*, H,0, heat acetyl chloride
#7) design synthesis for the following mechanism use image
You are given the following reactions to complete in lab. However, you recognize an issue with the reaction. 1. Determine why the reactions will not work or why the reactions will give a poor yield? 2. How can you resolve the issues and run the reactions to obtain a better yield? Fix the reactions by redrawing each reaction with the solution (corrected starting materials/reagents/products/etc.).
Answer 36 only!! 35 is for reference!!
Help me understand the break down of this reaction in sequence and a complete reaction scheme, thank you!