Relative Intensity Transmitance() 10 20 IR Spectrum Mass Spectrum 40 20 100 80 60- W 3500 3000 2500 Wavenumber (cm-1) 2000 1500 1000 500 [M+H]* -0 20 25 30 35 40 45 50 55 70 75 80 m/z b. 1H NMR (a broad singlet with 2H is observed at 6.2 ppm) 22 13C NMR 20 1.8 1.6 1.4 1.2 1.0 8 (ppm) 200 150 8 (ppm) 100 50
Relative Intensity Transmitance() 10 20 IR Spectrum Mass Spectrum 40 20 100 80 60- W 3500 3000 2500 Wavenumber (cm-1) 2000 1500 1000 500 [M+H]* -0 20 25 30 35 40 45 50 55 70 75 80 m/z b. 1H NMR (a broad singlet with 2H is observed at 6.2 ppm) 22 13C NMR 20 1.8 1.6 1.4 1.2 1.0 8 (ppm) 200 150 8 (ppm) 100 50
Principles of Instrumental Analysis
7th Edition
ISBN:9781305577213
Author:Douglas A. Skoog, F. James Holler, Stanley R. Crouch
Publisher:Douglas A. Skoog, F. James Holler, Stanley R. Crouch
Chapter19: Nuclear Magnetic Resonance Spectroscopy
Section: Chapter Questions
Problem 19.31QAP: The proton NMR spectrum in Figure 19.39 is for an organic compound containing a single atom of...
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Question
Use the spectrometric data below to elucidate a structure. They will be a combination of 1H NMR, 13C NMR, IR, and MS.
![Relative Intensity
Transmitance()
10
20
IR Spectrum
Mass Spectrum
40
20
100
80
60-
W
3500
3000
2500
Wavenumber (cm-1)
2000
1500
1000
500
[M+H]*
-0
20
25
30
35
40
45
50
55
70
75
80
m/z](/v2/_next/image?url=https%3A%2F%2Fcontent.bartleby.com%2Fqna-images%2Fquestion%2F875d8d1b-faa4-405e-b19a-cdd65bf10267%2F6d1c6ccc-4f9c-448d-8636-344ac43f432a%2Fxxche3_processed.png&w=3840&q=75)
Transcribed Image Text:Relative Intensity
Transmitance()
10
20
IR Spectrum
Mass Spectrum
40
20
100
80
60-
W
3500
3000
2500
Wavenumber (cm-1)
2000
1500
1000
500
[M+H]*
-0
20
25
30
35
40
45
50
55
70
75
80
m/z
Transcribed Image Text:b. 1H NMR (a broad singlet with 2H is observed at 6.2 ppm)
22
13C NMR
20
1.8
1.6
1.4
1.2
1.0
8 (ppm)
200
150
8 (ppm)
100
50
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