Asphalt Technology HW Lecture 5 From the thin film oven test, it was found the following results: Original Pen No. (from penetration test) Weight before heating (gm) Weight after heating (gm) Container No. 1 131 dmm 50.3 48.8 2 49.7 48.2 Find the loss in weight due to the effect of heat and air and determine the retained penetration if the penetration value of residue after thin film oven test was 112 dmm. Then compare the results with standards (Specification limits (EN 12607-1): Change of mass, ± 0.8% and retained penetration 2 43%. Solution: 1- Find the average weight before and after heating as shown in the following table: W1: Average weight before heating (gm) W2: Average weight after heating (gm) 2- Find the loss in weight of residue after thin film oven test is reported as the percentage by mass of the original sample = W1-W2 100 sample has an overall mass (loss or gain) W1 ? (> or or53 >50 246 >43 >37 Change of mass fabsolute value) hcrease in softening point - severity 1 s0.5 <0.5 <0.5 <0.5 S0.8 <0.8 s1.0 <8 <8 <8 <9 <10 <11 or or or or or or or or hcrease in softening point - severity 2 a Flosh point Solubility Panetration index C s10 s11 s11 s12 s12 EN ISO 2592 °C 2240 2240 2240 >230 >230 2230 >230 >220 EN 12592 299.0 299.0 299.0 299.0 299.0 299.0 299.0 299.0 Annex A b -1.5 to +0,7 Dynamic viscosity at 60°C Breaking point (Fraass) Kinematic viscosity at 135 C EN 12596 Pas >440 >260 >225 >175 >145 >90 >55 >30 EN 12593 <-5 <-7 <-8 <-10 <-12 <-15 EN 12595 mm/s 2530 2400 2370 2325 >295 2230 2175 2135 France Belgium The Netherlands Germany UK Switzerland Czech Republic Poland ae ae Y

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Publisher:KASSIMALI, Aslam.
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Asphalt Technology
HW
Lecture 5
From the thin film oven test, it was found the following results:
Container No.
Original Pen No.
(from penetration test)
Weight before
heating (gm)
Weight after
heating (gm)
1
131 dmm
50.3
48.8
2
49.7
48.2
Find the loss in weight due to the effect of heat and air and determine the retained penetration if the
penetration value of residue after thin film oven test was 112 dmm. Then compare the results with standards
(Specification limits (EN 12607-1): Change of mass, + 0.8% and retained penetration 2 43%.
Solution:
1- Find the average weight before and after heating as shown in the following table:
W1: Average weight before heating (gm)
W2: Average weight after heating (gm)
2- Find the loss in weight of residue after thin film oven test is reported as the percentage by mass of the
W1-W2
*100 = ? sample has an overall mass ? (Iloss or gain)
original sample =
W1
? (> or<or=) 0.8% (the max limit of EN standard).
3- Retained penetration ? (> or<or=) 43% (the limit of EN standard).
Table 5.1 Specifications for paving grade bitumens with penetrations from 20 x 0.1 mm to 220 x 0.1 mm: Tables 1A and 18 of EN 12591 combined, including
examples of specific regional requirements (BSI, 2009a)
Property
Test method
Unit
20/30
30/45
35/50
70/100 100/150 160/220
40/60
50/70
Penetration at 25°C
EN 1426
0.1 mm
20-30
30-45
35-50
40-60
50-70
70-100
100-150 160-220
Softening point
EN 1427
°C
55-63
52-60
50-58
48-56
46-54
43-51
39-47
35-43
Resistance to hardening at 163 C
EN 12607-1
Retained penetration
255
s0.5
>53
>53
<0.5
>50
250
>46
>43
>37
Change of mass (absolute value)
hcrease in softening point - severity 1
S0.5
<0.5
0.5
S0.8
<0.8
$1.0
<8
<8
<8
<9
<9
<10
<11
or
or
or
or
or
or
or
or
hcrease in softening point - severity 2 a
Flosh point
Solubility
Panetration index
s10
s11
s11
s11
s12
s12
EN ISO 2592
°C
2240
2240
2240
>230
>230
>230
2230
>220
EN 12592
299.0
299.0
299.0
299.0
299.0
299.0
299.0
299.0
Annex Ab
-1.5 to +0,7
Dynamic viscosity at 60°C
Breaking point (Fraass)
Kinematic viscosity at 135 C
EN 12596
Pa-s
>440
>260
>225
>175
>145
>90
>55
>30
EN 12593
<-5
<-5
<-7
-8
<-10
-12
-15
EN 12595
mm/s
2530
2400
2370
>325
>295
>230
2175
2135
France
Belgium
The Netherlands
Germany
UK
Switzerland
Czech Republic
Poland
ae ae Y
Transcribed Image Text:Asphalt Technology HW Lecture 5 From the thin film oven test, it was found the following results: Container No. Original Pen No. (from penetration test) Weight before heating (gm) Weight after heating (gm) 1 131 dmm 50.3 48.8 2 49.7 48.2 Find the loss in weight due to the effect of heat and air and determine the retained penetration if the penetration value of residue after thin film oven test was 112 dmm. Then compare the results with standards (Specification limits (EN 12607-1): Change of mass, + 0.8% and retained penetration 2 43%. Solution: 1- Find the average weight before and after heating as shown in the following table: W1: Average weight before heating (gm) W2: Average weight after heating (gm) 2- Find the loss in weight of residue after thin film oven test is reported as the percentage by mass of the W1-W2 *100 = ? sample has an overall mass ? (Iloss or gain) original sample = W1 ? (> or<or=) 0.8% (the max limit of EN standard). 3- Retained penetration ? (> or<or=) 43% (the limit of EN standard). Table 5.1 Specifications for paving grade bitumens with penetrations from 20 x 0.1 mm to 220 x 0.1 mm: Tables 1A and 18 of EN 12591 combined, including examples of specific regional requirements (BSI, 2009a) Property Test method Unit 20/30 30/45 35/50 70/100 100/150 160/220 40/60 50/70 Penetration at 25°C EN 1426 0.1 mm 20-30 30-45 35-50 40-60 50-70 70-100 100-150 160-220 Softening point EN 1427 °C 55-63 52-60 50-58 48-56 46-54 43-51 39-47 35-43 Resistance to hardening at 163 C EN 12607-1 Retained penetration 255 s0.5 >53 >53 <0.5 >50 250 >46 >43 >37 Change of mass (absolute value) hcrease in softening point - severity 1 S0.5 <0.5 0.5 S0.8 <0.8 $1.0 <8 <8 <8 <9 <9 <10 <11 or or or or or or or or hcrease in softening point - severity 2 a Flosh point Solubility Panetration index s10 s11 s11 s11 s12 s12 EN ISO 2592 °C 2240 2240 2240 >230 >230 >230 2230 >220 EN 12592 299.0 299.0 299.0 299.0 299.0 299.0 299.0 299.0 Annex Ab -1.5 to +0,7 Dynamic viscosity at 60°C Breaking point (Fraass) Kinematic viscosity at 135 C EN 12596 Pa-s >440 >260 >225 >175 >145 >90 >55 >30 EN 12593 <-5 <-5 <-7 -8 <-10 -12 -15 EN 12595 mm/s 2530 2400 2370 >325 >295 >230 2175 2135 France Belgium The Netherlands Germany UK Switzerland Czech Republic Poland ae ae Y
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