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A B HO Write the missing product or reagent in each of the following: HO OTBDPS NHBoc H N-Boc En 0. i-ProTMS, TMSOTY, CH₂Cl₂ It, 24 h 0 (Hint: Think of TMS as a big proton. These conditions are dehydrating.) Olde D HOH C Ome =Ph (DHQ)₂PHAL (0.01 eq) K₂ Os 042H₂0 (0.005 eq) K₂Fe(CN) (3 eq) K₂CO, (3 eq) CH₂SO₂NH₂ (1 eq) t-BuOH:H₂0 (1:1) 0°C, 22 h DMSO, (COCI), CH₂Cl₂ E₂N, -78°C to It G A B E TBAF, THF, 3 h, it Ade, C(Ode) (4 eq) TsOHH₂0 (0.05 eq) CH₂Cl₂, 50°C, 25 h F

A B HO Write the missing product or reagent in each of the following: HO OTBDPS NHBoc H N-Boc En 0. i-ProTMS, TMSOTY, CH₂Cl₂ It, 24 h 0 (Hint: Think of TMS as a big proton. These conditions are dehydrating.) Olde D HOH C Ome =Ph (DHQ)₂PHAL (0.01 eq) K₂ Os 042H₂0 (0.005 eq) K₂Fe(CN) (3 eq) K₂CO, (3 eq) CH₂SO₂NH₂ (1 eq) t-BuOH:H₂0 (1:1) 0°C, 22 h DMSO, (COCI), CH₂Cl₂ E₂N, -78°C to It G A B E TBAF, THF, 3 h, it Ade, C(Ode) (4 eq) TsOHH₂0 (0.05 eq) CH₂Cl₂, 50°C, 25 h F

Chemistry
Chemistry
10th Edition
ISBN:9781305957404
Author:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Publisher:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Chapter1: Chemical Foundations
Section: Chapter Questions
Problem 1RQ: Define and explain the differences between the following terms. a. law and theory b. theory and...
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A B HO Write the missing product or reagent in each of the following: HO OTBDPS NHBoc H N-Boc En 0, i-ProTMS, TMSOTY, CH₂Cl₂ It, 24 h 0 (Hint: Think of TMS as a big proton. These conditions are dehydrating.) Olde D H OH C Ome =Ph (DHQ)₂PHAL (0.01 eq) K₂ Os 042H₂0 (0.005 eq) K₂Fe(CN) (3 eq) K₂CO, (3 eq) CH₂SO₂NH₂ (1 eq) t-BuOH:H₂0 (1:1) 0°C, 22 h DMSO, (COCI), CH₂Cl₂ E₂N, -78°C to It G A B E TBAF, THF, 3 h, it Ade, C(Ode) (4 eq) TsOHH₂0 (0.05 eq) CH₂Cl₂, 50°C, 25 h F
Transcribed Image Text:A B HO Write the missing product or reagent in each of the following: HO OTBDPS NHBoc H N-Boc En 0, i-ProTMS, TMSOTY, CH₂Cl₂ It, 24 h 0 (Hint: Think of TMS as a big proton. These conditions are dehydrating.) Olde D H OH C Ome =Ph (DHQ)₂PHAL (0.01 eq) K₂ Os 042H₂0 (0.005 eq) K₂Fe(CN) (3 eq) K₂CO, (3 eq) CH₂SO₂NH₂ (1 eq) t-BuOH:H₂0 (1:1) 0°C, 22 h DMSO, (COCI), CH₂Cl₂ E₂N, -78°C to It G A B E TBAF, THF, 3 h, it Ade, C(Ode) (4 eq) TsOHH₂0 (0.05 eq) CH₂Cl₂, 50°C, 25 h F
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