A 0.2400 g rock sample containing an unknown amount of Ca was dissolved in HCl and diluted to 100.0 mL. Aliquots of 15.00 mL from this solution were added to different volumes of a 2.08 µg/mL Ca standard solution and diluted to 200.0 mL. The emission intensity of these solutions was measured using atomic emission spectroscopy. The results are shown in the table. Unknown volume (mL) Standard volume (mL) Final volume (mL) Emission Intensity 15.00 0.00 200.0 204.0 15.00 5.00 200.0 390.0 15.00 10.00 200.0 614.0 15.00 15.00 200.0 808.0 15.00 20.00 200.0 998.0 Find the weight percent of Ca in the rock sample and its uncertainty using the method of standard additions. weight percent: % Ca %

Introduction to Chemical Engineering Thermodynamics
8th Edition
ISBN:9781259696527
Author:J.M. Smith Termodinamica en ingenieria quimica, Hendrick C Van Ness, Michael Abbott, Mark Swihart
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A 0.2400 g rock sample containing an unknown amount of Ca was dissolved in HCl and diluted to 100.0 mL. Aliquots of
15.00 mL from this solution were added to different volumes of a 2.08 µg/mL Ca standard solution and diluted to
200.0 mL. The emission intensity of these solutions was measured using atomic emission spectroscopy. The results are
shown in the table.
Unknown volume (mL) Standard volume (mL) Final volume (mL) Emission Intensity
15.00
0.00
200.0
204.0
15.00
5.00
200.0
390.0
15.00
10.00
200.0
614.0
15.00
15.00
200.0
808.0
15.00
20.00
200.0
998.0
Find the weight percent of Ca in the rock sample and its uncertainty using the method of standard additions.
weight percent:
% Ca
%
Transcribed Image Text:A 0.2400 g rock sample containing an unknown amount of Ca was dissolved in HCl and diluted to 100.0 mL. Aliquots of 15.00 mL from this solution were added to different volumes of a 2.08 µg/mL Ca standard solution and diluted to 200.0 mL. The emission intensity of these solutions was measured using atomic emission spectroscopy. The results are shown in the table. Unknown volume (mL) Standard volume (mL) Final volume (mL) Emission Intensity 15.00 0.00 200.0 204.0 15.00 5.00 200.0 390.0 15.00 10.00 200.0 614.0 15.00 15.00 200.0 808.0 15.00 20.00 200.0 998.0 Find the weight percent of Ca in the rock sample and its uncertainty using the method of standard additions. weight percent: % Ca %
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