8a. [8] Reactant R 8b. Describe from each what peaks correspond to the structures. [12] i. IR Spectrum ii. Mass Spectrum iii. 1H NMR iv. 13C NMR Product P 8. Use the spectrometric data to identify the type and write the reaction. [20] Reactant R IR Spectrum 1H NMR 3500 3000 2500 3.5 3.0 IR Spectrum 1H NMR qt 3500 2000 1500 1000 Wavenumber (cm) 2.5 8(ppm) 2500 Wavenumber (cm) Mass Spectrum RI 13C NMR 135.989 137.987 136.992 138.99 m/z 2.0 1.5 1.0 50 40 8(ppm) 30 20 Product Mass Spectrum 2000 1500 1000 500 dq RI 13C NMR 83.073 84.077 85.087 m/z 3.0 1.0 2.5 120 100 80 8(ppm) 60 40 20 8(ppm)
8a. [8] Reactant R 8b. Describe from each what peaks correspond to the structures. [12] i. IR Spectrum ii. Mass Spectrum iii. 1H NMR iv. 13C NMR Product P 8. Use the spectrometric data to identify the type and write the reaction. [20] Reactant R IR Spectrum 1H NMR 3500 3000 2500 3.5 3.0 IR Spectrum 1H NMR qt 3500 2000 1500 1000 Wavenumber (cm) 2.5 8(ppm) 2500 Wavenumber (cm) Mass Spectrum RI 13C NMR 135.989 137.987 136.992 138.99 m/z 2.0 1.5 1.0 50 40 8(ppm) 30 20 Product Mass Spectrum 2000 1500 1000 500 dq RI 13C NMR 83.073 84.077 85.087 m/z 3.0 1.0 2.5 120 100 80 8(ppm) 60 40 20 8(ppm)
Principles of Instrumental Analysis
7th Edition
ISBN:9781305577213
Author:Douglas A. Skoog, F. James Holler, Stanley R. Crouch
Publisher:Douglas A. Skoog, F. James Holler, Stanley R. Crouch
Chapter11: Atomic Mass Spectrometry
Section: Chapter Questions
Problem 11.2QAP
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