70- H3CO. NH2 Cr H3Co C,H19CIN,O, Mol. Wt. 350.79676 3800 3600 3400 3200 3000 2800 2600 2400 2200 2000 1800 1600 1400 1200 1000 800 Wavenumber 3018- 2918- 2727 oze 2488 1518 T416 1119- 1018- 196 600 192
70- H3CO. NH2 Cr H3Co C,H19CIN,O, Mol. Wt. 350.79676 3800 3600 3400 3200 3000 2800 2600 2400 2200 2000 1800 1600 1400 1200 1000 800 Wavenumber 3018- 2918- 2727 oze 2488 1518 T416 1119- 1018- 196 600 192
Chemistry
10th Edition
ISBN:9781305957404
Author:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Publisher:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Chapter1: Chemical Foundations
Section: Chapter Questions
Problem 1RQ: Define and explain the differences between the following terms. a. law and theory b. theory and...
Related questions
Question
How do I analyse whether product isoquinoline has been synthesised through IR spectrum?

Transcribed Image Text:90
7아
H3CO.
6아
NH2 Cr
H3co
5아
O2N
9
4아
C1,H19CIN,0,
Mol. Wt.: 350.79676
3아
2아
3800
3600
3400
3200
3000
2800
2600
2400
2200
2000
1800
1600
1400
1200
1000
800
Wavenumber
%Transmitance
3018-
2918-
2727-
2620
2533-
2488
1518-
1453
1416-
348
1303-
1119
1058-
1018-
914
863
609
761-
732-
689

Transcribed Image Text:The Experiment
In this experiment, isoquinoline 9 will be synthesised, according to Scheme 4. The Schiff base 8 is
prepared by the condensation of 3,4-dimethylphenethylamine 6 with 3-nitrobenzaldehyde 7. The
cyclisation of the Schiff base 8, under strong acid conditions, would provide the Hcl salt of isoquinoline
9.
H3CO.
H,CO.
H3CO
H,CO
NH2
ethanol
con. HCI
NH2 Cr
H3CO
H3CO
40°C
reflux
H.
O,N
O,N
Schiff base 8
7
NO,
Scheme 4
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