70- H3CO. NH2 Cr H3Co C,H19CIN,O, Mol. Wt. 350.79676 3800 3600 3400 3200 3000 2800 2600 2400 2200 2000 1800 1600 1400 1200 1000 800 Wavenumber 3018- 2918- 2727 oze 2488 1518 T416 1119- 1018- 196 600 192

Chemistry
10th Edition
ISBN:9781305957404
Author:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Publisher:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Chapter1: Chemical Foundations
Section: Chapter Questions
Problem 1RQ: Define and explain the differences between the following terms. a. law and theory b. theory and...
icon
Related questions
Question

How do I analyse whether product isoquinoline has been synthesised through IR spectrum? 


90
7아
H3CO.
6아
NH2 Cr
H3co
5아
O2N
9
4아
C1,H19CIN,0,
Mol. Wt.: 350.79676
3아
2아
3800
3600
3400
3200
3000
2800
2600
2400
2200
2000
1800
1600
1400
1200
1000
800
Wavenumber
%Transmitance
3018-
2918-
2727-
2620
2533-
2488
1518-
1453
1416-
348
1303-
1119
1058-
1018-
914
863
609
761-
732-
689
Transcribed Image Text:90 7아 H3CO. 6아 NH2 Cr H3co 5아 O2N 9 4아 C1,H19CIN,0, Mol. Wt.: 350.79676 3아 2아 3800 3600 3400 3200 3000 2800 2600 2400 2200 2000 1800 1600 1400 1200 1000 800 Wavenumber %Transmitance 3018- 2918- 2727- 2620 2533- 2488 1518- 1453 1416- 348 1303- 1119 1058- 1018- 914 863 609 761- 732- 689
The Experiment
In this experiment, isoquinoline 9 will be synthesised, according to Scheme 4. The Schiff base 8 is
prepared by the condensation of 3,4-dimethylphenethylamine 6 with 3-nitrobenzaldehyde 7. The
cyclisation of the Schiff base 8, under strong acid conditions, would provide the Hcl salt of isoquinoline
9.
H3CO.
H,CO.
H3CO
H,CO
NH2
ethanol
con. HCI
NH2 Cr
H3CO
H3CO
40°C
reflux
H.
O,N
O,N
Schiff base 8
7
NO,
Scheme 4
Transcribed Image Text:The Experiment In this experiment, isoquinoline 9 will be synthesised, according to Scheme 4. The Schiff base 8 is prepared by the condensation of 3,4-dimethylphenethylamine 6 with 3-nitrobenzaldehyde 7. The cyclisation of the Schiff base 8, under strong acid conditions, would provide the Hcl salt of isoquinoline 9. H3CO. H,CO. H3CO H,CO NH2 ethanol con. HCI NH2 Cr H3CO H3CO 40°C reflux H. O,N O,N Schiff base 8 7 NO, Scheme 4
Expert Solution
trending now

Trending now

This is a popular solution!

steps

Step by step

Solved in 2 steps

Blurred answer
Similar questions
  • SEE MORE QUESTIONS
Recommended textbooks for you
Chemistry
Chemistry
Chemistry
ISBN:
9781305957404
Author:
Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Publisher:
Cengage Learning
Chemistry
Chemistry
Chemistry
ISBN:
9781259911156
Author:
Raymond Chang Dr., Jason Overby Professor
Publisher:
McGraw-Hill Education
Principles of Instrumental Analysis
Principles of Instrumental Analysis
Chemistry
ISBN:
9781305577213
Author:
Douglas A. Skoog, F. James Holler, Stanley R. Crouch
Publisher:
Cengage Learning
Organic Chemistry
Organic Chemistry
Chemistry
ISBN:
9780078021558
Author:
Janice Gorzynski Smith Dr.
Publisher:
McGraw-Hill Education
Chemistry: Principles and Reactions
Chemistry: Principles and Reactions
Chemistry
ISBN:
9781305079373
Author:
William L. Masterton, Cecile N. Hurley
Publisher:
Cengage Learning
Elementary Principles of Chemical Processes, Bind…
Elementary Principles of Chemical Processes, Bind…
Chemistry
ISBN:
9781118431221
Author:
Richard M. Felder, Ronald W. Rousseau, Lisa G. Bullard
Publisher:
WILEY