5. After recrystallizing a compound from toluene (BP 110 °C), Alex finds that the mass of the crystals keeps decreasing at a rate of ~1 mg per second on a balance. Alex decides to check the melting point of the crystals while waiting for the balance to stabilize, but gets a lowered and broadened temperature range compared to the expected melting point. What advice do you have for Alex? Identify the problem Alex is facing and a possible solution in your advice.

Chemistry
10th Edition
ISBN:9781305957404
Author:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Publisher:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Chapter1: Chemical Foundations
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5. After recrystallizing a compound from toluene (BP 110 °C), Alex finds that
the mass of the crystals keeps decreasing at a rate of ~1 mg per second on a
balance. Alex decides to check the melting point of the crystals while waiting
for the balance to stabilize, but gets a lowered and broadened temperature
range compared to the expected melting point. What advice do you have for
Alex? Identify the problem Alex is facing and a possible solution in your
advice.
6. In a recrystallization, why is it important to dissolve the solute in boiling
solvent instead of cold solvent?
To melt the solute
To boil the solute
To use as small amount of solvent to dissolve the soluté as possible
Transcribed Image Text:2/5 — 100% + piration=16/140. 5. After recrystallizing a compound from toluene (BP 110 °C), Alex finds that the mass of the crystals keeps decreasing at a rate of ~1 mg per second on a balance. Alex decides to check the melting point of the crystals while waiting for the balance to stabilize, but gets a lowered and broadened temperature range compared to the expected melting point. What advice do you have for Alex? Identify the problem Alex is facing and a possible solution in your advice. 6. In a recrystallization, why is it important to dissolve the solute in boiling solvent instead of cold solvent? To melt the solute To boil the solute To use as small amount of solvent to dissolve the soluté as possible
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