4. Often we will ask that you scale your procedure up or down, meaning we will change the amounts of material we will use. The following is a procedure as written in an organic lab experiment. Write the procedure out as if you were asked to scale up by a factor of 2. Make any necessary changes to equipment sizes, reaction times, etc. Remember that you should never heat a reaction vessel that is more than ½ full. "In a 50 mL round-bottom flask place 2 grams of compound X and 15 mL of benzene. Reflux the reaction for 30 minutes. After the reaction has cooled, add 10 mL of ice-cold water. Collect the product by vacuum filtration and wash it with two 10 mL portions of ice-cold water."

4. Often we will ask that you scale your procedure up or down, meaning we will change the amounts of material we will use. The following is a procedure as written in an organic lab experiment. Write the procedure out as if you were asked to scale up by a factor of 2. Make any necessary changes to equipment sizes, reaction times, etc. Remember that you should never heat a reaction vessel that is more than ½ full. "In a 50 mL round-bottom flask place 2 grams of compound X and 15 mL of benzene. Reflux the reaction for 30 minutes. After the reaction has cooled, add 10 mL of ice-cold water. Collect the product by vacuum filtration and wash it with two 10 mL portions of ice-cold water."

Chemistry

10th Edition

ISBN:9781305957404

Author:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste

Publisher:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste

Chapter1: Chemical Foundations

Section: Chapter Questions

Problem 1RQ: Define and explain the differences between the following terms. a. law and theory b. theory and...

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After a complicated chemical synthesis, the last step is to separate two liquids, ACETONE AND ANILINE. What separation method should you use? (Feel free to access the SDS for the two compounds). Be specific about the exact type of separation you choose and explain why.
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