2C. Write the separation scheme for the isolation of triphenylmethanol from the reaction mixture once the reaction is complete. The separation begins after the addition of HCI and water to the reaction and includes the column chromatography procedure to further purify crude triphenylmethanol isolated in the day 1 procedure.
2C. Write the separation scheme for the isolation of triphenylmethanol from the reaction mixture once the reaction is complete. The separation begins after the addition of HCI and water to the reaction and includes the column chromatography procedure to further purify crude triphenylmethanol isolated in the day 1 procedure.
Chemistry
10th Edition
ISBN:9781305957404
Author:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Publisher:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Chapter1: Chemical Foundations
Section: Chapter Questions
Problem 1RQ: Define and explain the differences between the following terms. a. law and theory b. theory and...
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Answer 2c
answer must be typed/digitally illustrated if applicable (cannot be hand drawn - it will be marked as incorrect if it is hand drawn)
Transcribed Image Text:2A. What is the theoretical yield and limiting reagent for the reaction to form triphenylmethanol in the
experiment provided if the reaction is started with 0.6 g of magnesium, 2.3 mL of bromobenzene, 3.75 g
benzophenone, and 17 mL of diethyl ether (total)?
2B. The Grignard reagent is very water sensitive. What are the procedures used in the experiment
provided to prevent exposure of the Grignard reagent to water? What will happen if those procedures
are not followed?
2C. Write the separation scheme for the isolation of triphenylmethanol from the reaction mixture once
the reaction is complete. The separation begins after the addition of HCI and water to the reaction and
includes the column chromatography procedure to further purify crude triphenylmethanol isolated in the
day 1 procedure.
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