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136 PRACTICAL SPECTROSCOPY Compound 78 is a high-boiling liquid (boiling point 189° C) that contains halogen, but will not react with alkoxides to yield an halogen. ether. The Mass, IR, and 'H NMR spectra, along with 13C NMR data, are given below. Elemental Analysis: C, 35.32; H, 2.47; contains "C Spectral Data: doublet, 137.4 ppm; doublet, 130.1 ppm; doublet, 127.4 ppm; singlet, 97.3 ppm Absorbance Mass Spectrum Intensity 204 77 128 40 80 20 100 120 140 160 m/e 180 200 220 240 260 280 300 Infrared Spectrum Wave Number, cm*1 4000 3000 2500 2000 1500 1300 1200 1100 1000 900 800 700 18 3 5 6 'H NMR 1 B 9 10 11 12 13 15 Wavelength, microns 6 5 4 3 ppm, 6 Structure: C2000 Brooks/Cole Publishing Com

136 PRACTICAL SPECTROSCOPY Compound 78 is a high-boiling liquid (boiling point 189° C) that contains halogen, but will not react with alkoxides to yield an halogen. ether. The Mass, IR, and 'H NMR spectra, along with 13C NMR data, are given below. Elemental Analysis: C, 35.32; H, 2.47; contains "C Spectral Data: doublet, 137.4 ppm; doublet, 130.1 ppm; doublet, 127.4 ppm; singlet, 97.3 ppm Absorbance Mass Spectrum Intensity 204 77 128 40 80 20 100 120 140 160 m/e 180 200 220 240 260 280 300 Infrared Spectrum Wave Number, cm*1 4000 3000 2500 2000 1500 1300 1200 1100 1000 900 800 700 18 3 5 6 'H NMR 1 B 9 10 11 12 13 15 Wavelength, microns 6 5 4 3 ppm, 6 Structure: C2000 Brooks/Cole Publishing Com

Macroscale and Microscale Organic Experiments
Macroscale and Microscale Organic Experiments
7th Edition
ISBN:9781305577190
Author:Kenneth L. Williamson, Katherine M. Masters
Publisher:Kenneth L. Williamson, Katherine M. Masters
Chapter13: Mass Spectrometry
Section: Chapter Questions
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136 PRACTICAL SPECTROSCOPY Compound 78 is a high-boiling liquid (boiling point 189° C) that contains halogen, but will not react with alkoxides to yield an halogen. ether. The Mass, IR, and 'H NMR spectra, along with 13C NMR data, are given below. Elemental Analysis: C, 35.32; H, 2.47; contains "C Spectral Data: doublet, 137.4 ppm; doublet, 130.1 ppm; doublet, 127.4 ppm; singlet, 97.3 ppm Absorbance Mass Spectrum Intensity 204 77 128 40 80 20 100 120 140 160 m/e 180 200 220 240 260 280 300 Infrared Spectrum Wave Number, cm*1 4000 3000 2500 2000 1500 1300 1200 1100 1000 900 800 700 18 3 5 6 'H NMR 1 B 9 10 11 12 13 15 Wavelength, microns 6 5 4 3 ppm, 6 Structure: C2000 Brooks/Cole Publishing Com
Transcribed Image Text:136 PRACTICAL SPECTROSCOPY Compound 78 is a high-boiling liquid (boiling point 189° C) that contains halogen, but will not react with alkoxides to yield an halogen. ether. The Mass, IR, and 'H NMR spectra, along with 13C NMR data, are given below. Elemental Analysis: C, 35.32; H, 2.47; contains "C Spectral Data: doublet, 137.4 ppm; doublet, 130.1 ppm; doublet, 127.4 ppm; singlet, 97.3 ppm Absorbance Mass Spectrum Intensity 204 77 128 40 80 20 100 120 140 160 m/e 180 200 220 240 260 280 300 Infrared Spectrum Wave Number, cm*1 4000 3000 2500 2000 1500 1300 1200 1100 1000 900 800 700 18 3 5 6 'H NMR 1 B 9 10 11 12 13 15 Wavelength, microns 6 5 4 3 ppm, 6 Structure: C2000 Brooks/Cole Publishing Com
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