1) Zn e) Br OCH,CH CH/CH)CH 2) acidify cold 1) LIAIH, (excess) OCH THE / O°C -n PHCH,0 2) Nalo, / THE H,0 pH 7 buffer TKO'P), (0,1 eg) (DET (0.1 eg 9) OH 'BUOOH (3.0 eg) CH,Cl, /-23°C/ 18 h
1) Zn e) Br OCH,CH CH/CH)CH 2) acidify cold 1) LIAIH, (excess) OCH THE / O°C -n PHCH,0 2) Nalo, / THE H,0 pH 7 buffer TKO'P), (0,1 eg) (DET (0.1 eg 9) OH 'BUOOH (3.0 eg) CH,Cl, /-23°C/ 18 h
Chemistry
10th Edition
ISBN:9781305957404
Author:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Publisher:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Chapter1: Chemical Foundations
Section: Chapter Questions
Problem 1RQ: Define and explain the differences between the following terms. a. law and theory b. theory and...
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Question
![1) Zn
Br
OCH,CH CH(CHolCH
2) acidify cold
1) LIAIH, (excess)
THE / O°C -nt
OCH,
PHCH;0
2) Nalo, / THF
H20 pH 7 buffer
TI(O'Pr), (0.1 ea)
9)
(-+DET (0.1 eg
'BUOOH (3.0 eg)
CH,C, /-23°C/ 18 h
OH
h)
N(CHo2
LIAIH, / Ether
35°C/ 15h
3-
3.
MgBr / Cul
os(CH2
THE / -78°C - it
2) 'Bu(CH3),SICI/ imidazole
DMAP / CH,C, it
i)
Oso, (0.6 eg)
Ba(CIO32](/v2/_next/image?url=https%3A%2F%2Fcontent.bartleby.com%2Fqna-images%2Fquestion%2F5c427e9d-efd5-4df5-a382-a68b07c6a036%2Ffe312bbf-5bb7-45e2-9e8e-60d4577356d9%2Fcdhlfkf_processed.jpeg&w=3840&q=75)
Transcribed Image Text:1) Zn
Br
OCH,CH CH(CHolCH
2) acidify cold
1) LIAIH, (excess)
THE / O°C -nt
OCH,
PHCH;0
2) Nalo, / THF
H20 pH 7 buffer
TI(O'Pr), (0.1 ea)
9)
(-+DET (0.1 eg
'BUOOH (3.0 eg)
CH,C, /-23°C/ 18 h
OH
h)
N(CHo2
LIAIH, / Ether
35°C/ 15h
3-
3.
MgBr / Cul
os(CH2
THE / -78°C - it
2) 'Bu(CH3),SICI/ imidazole
DMAP / CH,C, it
i)
Oso, (0.6 eg)
Ba(CIO32
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