1 a) Provide a detailed experimental report for the preparation, analysis and results (Theoretical and percent yield calculations etc) that you will need to employ for the preparation of 2 grams of para nitroacetanilde from 2 grams of acetanilide. b) Include amounts of any other reagents that are needed, safety precautions that should be followed for the synthesis.

Q: (c) (d) 15.7 Complete these reactions involving lithium diorganocopper (Gilman) reagents (b) D. CuLi…

A: An arrow always depicts from a region of high electron density to low electron density ; that is…

Q: 4. When the compound represented by the structural formula is warıned with aqueous solution of…

A: Ester hydrolysis reaction: In the ester hydrolysis reaction, the ester is converted into carboxylic…

Q: Write the mechanisms of reaction for the formation of acetanilide from aniline and acetic anhydride

A:

Q: 4. Synthesize the following compound. You may use benzene, acetylene, ethanol and any inorganic…

A: First ethanol to ethyl bromide then start with benzene to form ethyl benzene which undergoes…

Q: In section (ii) above an acetal group is present in the starting material. Give a general reaction…

A: An acetyl is an organic compound formed by the addition of two hydroxyl group on an aldehyde or a…

Q: Is the crude (non-crystallized) acetanilide pure? Why or why not?  Is the crystallized acetanilide…

A: Any crude compound like acetanilide can't be ultra pure . Because it contain lots of impurities…

Q: Substantially discuss how Nitration of Toluene works

A: Toluene gives ortho and para isomer by the nitration,but it heated it can be give dinitro toluene…

Q: Explain and describe  objective for preparation of methyl orange?

A: Methyl orange is a pH indicator. It has two distinct forms. Red in acidic medium and yellow in basic…

Q: The question is: Provide a method for separating a mixture of benzophenone and tributylamine which…

A: The mixture of Benzophenone and tributylamine in diethyl ether taken in a separating funnel then…

Q: Outline an extraction procedure by which you would separate a mixture of the following three…

A: Step 1 : mixture of compounds is treated with 10% HCl, aniline will go into water layer. water layer…

Q: Explain why it is possible to separate a mixture of p-nitrobenzoic acid and ethyl phenyl ether…

A: We are given a mixture of p-nitrobenzoic acid and ethyl phenyl ether, and we have to separate this…

Q: Write an essay  for  the Synthesis of P-Nitroaniline,  a 100 gram of acetanilide,  1mL of sulfuric…

A: Aim: To prepare p-nitroaniline from the given 100 g acetaniline Chemicals required: acetaanilide,…

Q: Working in a fume hood, to 1 cm of the organic compound in a test tube add On addition of PCLS fumes…

A: The test is based upon the reaction of an organic compound with PCl5.

Q: Draw reaction mechanisms, using curved arrows to show the flow of electrons, for the acid-base…

A: The question is based on the concept of separation of compounds. We need to write mechanism for acid…

Q: 3. Suggest synthesis routes for the following conversions. Include brief reaction conditions.

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Q: Provide detailed explanation and analysis for preparation of methyl orange.

A: Methyl orange is used as dye.

Q: 2. Please explain what is A and B in the separating funnel when using NaOH to extract…

A: Extraction is a separation technique use to separate any compound from mixture. Common extraction…

Q: Question 1: (a) pK, of 4-methoxybenzenethiol was measured in DMSO, water, MeOH and MeOH/water…

A: Water will make it more acidic because water is a polar solvent it stablise the given compound after…

Q: Write a cleare scientific prosedure of preparing p-creaol from phenol in laboratory, what is the…

A: A chemical reaction is a mechanism that converts one or more substances, known as reactants, into…

Q: Electrophilic aromatic substitution is a general reaction of aromatic compounds, including…

A: Sulfuric acid and nitric acid combine to give NO2+ as an electrophile.

Q: You have been given a mixture of toluene,aniline and benzoic acid dissolved in chloroform.explain in…

A:

Q: Someone decided to try to recrystallize the molecule biphenyl using benzene as a solvent, but…

A: Introduction Purifying solid substances through recrystallization is a method. 1 In comparison to…

Q: Please

A: We will choose correct option

Q: Obtain by synthesis the compound 3-phenylpropanoic acid by an acetylacetic or malonic synthesis.…

A: Malonic ester synthesis is a convenient method for synthesis of a carboxylic acid bearing an alkyl…

Q: Part 2. Recrystallization and Extraction. (a) Provide the two important characteristics of a good…

A: Please find your solution below : Recrystallization is an important technique used to purify…

Q: You are employed as a coop student at the Drug and Alcohol Testing Association of Canada (DATAC)…

A:

Q: Sample Identity and Rationalization

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Q: Н н НН нн н H

A: Cubane is a platonic hydrocarbon with 8 carbon atoms (C8H8) arranged in the form of a cube.

Q: Suggest a retrosynthetic analysis and synthesis for the moloCuloc given in thec e gUection V ou

A: When ethyl benzoate hydrolysis under alkaline condition followed by acidification gives benzoic acid…

Q: (a) 3-Methyl-2-pentanone is condensed with acetophenone in an alkaline medium (b)…

A:

Q: 1. What is the merchanism of synthesis of salicylamide?

A: Salicylamide: It is a derivative of salicylic acid. It can be synthesized from phenol or directly…

Q: What is the difference between the catalyzed and uncatalyzed preparation of acetanilide (acetic acid…

A: When acetanilide is prepared by reacting between aniline and acetic anhydride then here…

Q: Suggest a retrosynthetic analysis and synthesis for these molecule. OH но, HO.

A: The retrosynthesis is done for any molecule by looking the several factors like electronic…

Q: OMe OMe

A:

Q: Compound X was soluble in water and ether, and its aqueous solution turned litmus blue. It reacted…

A:

Q: Follow the detailed instructions provided in each of the subsections (a-b): a) Fill in the following…

A: Carboxylic acid is converted into acid chloride by treated with SOCl2  Carboxylic acid is…

Q: Give Four main precautions need to be considered when carrying out the following. b) Synthesis of…

A: Benzopinacole (white color precipitate) generation is done via photoreduction method. It is highly…

Q: (a) A useful synthesis of some diols includes the reaction of "bis-Grignard" reagents (compounds…

A: Organic  reactions:

Q: Present a synthetic route reported in the literature for the synthesis of the captopril from…

A: Introduction: Captopril is a drug used for hypertension and heart failure. Basically it is an…

Q: You are given a mixture containing the three compounds shown below. Outline a procedure for the…

A:

NMR Spectroscopy

NMR stands for Nuclear Magnetic Resonance in which the study of different molecules is done based on the interaction of radiofrequency electromagnetic radiations with the nuclei of molecules placed in a strong magnetic field. A precise study of spectra of visible light and all bands of electromagnetic radiation is called spectroscopy.