LAB REPORT MODULE 5

7. You can see an MSDS below. Please answer the following questions related to the MSDS. a) What is the name of this chemical? b) What should you do if someone drinks the chemical? c) Would this chemical catch on fire if it was exposed to flames? d) If this chemical gets in your eye what should you do? e) What color is this chemical? f) What should you do if someone spills a small amount of the chemical?

PART ONE: Preparation of FECNS* Solution Prepare the two solutions in table 1 by accurately measuring the required volumes of distilled water and CNS into two labeled test tubes. The absorbance of the solutions must be measured soon after adding the Fe" solution from a buret. TABLE 1 Fe 5 ml 5S mL Solution Distilled Water CNS 2 mL Total Volume 3 ml 2 ml 10 ml 3 mL 10 ml In this part of the experiment you are to explore what the above quote means. As a PRELIMINARY Exercise, formulate a hypothesis as to what would happen under each of the following circumstances: 1. 1ml of 0.0020 M CNS' solution is added to the unused portion of solution 1 in the test tube 2. One drop of 0.20 M CNS solution is added to the unused portion of solution 2 in the test tube.

Dangerous Paint Stripper Jessica has a summer job working for the city parks program. She has been using a cleaner called “Graffiti Gone” to remove graffiti from the bathrooms. She has to take a lot of breaks, because the chemical makes her throat burn. It also makes her feel dizzy sometimes, especially when the bathrooms don’t have very many windows. On the label, she sees that the cleaner has methylene chloride in it. She feels like she’s managing to get the work done, but she is worried about feeling dizzy. She wants to find out more about this chemical, what harm it can cause, and whether there are safer ways to do this work. Questions for following story. 1. What went right in this situation? 2. What went wrong in this situation? 3. What steps should be taken in this workplace to make sure employees are better protected and prepared the next time?

Analytical Chemistry Laboratory Experiment: Determination of Iron Content in Water Samples by Visible Spectroscopy

In a chromatography experiment, samples can be separated based on their polarity. If you have a polar solvent and nonpolar chromatography sheet, what conclusion can be drawn from analyzing the results? A. The sample that travels farthest up the sheet is most like the solvent, therefore it must be polar. B. The sample that travels farthest up the sheet is most like the solvent, therefore it must be nonpolar. C. The sample that doesn't travel at all and stays near the origin is most like the sheet, therefore it must be polar.  D. The sample that doesn't travel at all and stays near the origin is most like the solvent, therefore it must be polar.

Using Table 2.1, calculate the required amount (in g) of ammonium sulfate to bring the solution from 40% to 60% saturation.

Which of the following will give a negative deviation to Beers Law?  I. polychromatic radiation II. presence of stray light III. presence of particulates on the sample A. I and II only        B. II and III only        C. I and III only       D. I only

Choose the most accurate descriptions about quantitative analysis using atomic absorption spectrophotometer (AAS). A. The sample was digested with a concentrated acid, the digested solutions were diluted in 10x dilution factor and then was directly injected into AAS. B. AAS instrument can detect elements present only in solid samples C. Desolvation, vaporization, combustion, atomization, and ionization are the processes involved during sample analysis. D. Hollow cathode lamps (HCL) are energy sources that a cathode is made from a platinum element in a glass envelope of an inert filler gas. AAS is the most widely used instrumentation for the analysis of metal and traces metal samples. State one factor from the following is insignificant to AAS. A. Wide range sample analysis B. Effective C. Low cost D. Robust

I don't know these one

Table 1. Data on EDTA Standardization Weight of CaCO3 (g): 0.2003g Trial Volume of EDTA (mL) Molarity of EDTA (M) 1 8.60 2 8.50 8.55 Average Molarity of EDTA (M)

PART 3- LABORATORY EQUIPMENT EQUIPMENT NAME FUNCTION To hold test tubes. Attaches to a retort stand to support glassware being heated. To pour liquid from a large container into a small container. To provide a flame during an experiment. ones To light the Bunsen burner. To attach test tubes to a retort stand. To clean substances out of a test tube. To hold a hot crucible or flask. To hold a hot test tube. To place on the lab bench to prevent burning or to use with ring clamp. To transfer small amounts of liquid. To grow bacteria or contain small experiments. To hold liquids. To measure liquids. To contain experiments (a stopper can be used to close the flask). To hold a hot beaker. To perform an experiment with a different substance in each well. To hold chemicals and perform experiments in. To scoop and transfer small amounts of substances, To stir during experiments that involve mixing or dissolving.

Number 2,3,and 4

Need help filling this out. It is the Data Sheet for Ch. 2 Qualitative Analysis. Very much appreciated!

Absorbance 1.40 Beer's Law Plot 1.20 1.00 0.80 0.60 0.40 0.20 0.00 0 10 20 30 40 50 Concentration (M x 105) D The slope for the line is 80.23. Use the Beer's Law plot provided to determine the concentration for a solution with absorbance = 0.5786. M

Please help me graph this on a graph like this .

PLEASE DO HELP ME.. NO NEED FOR EXPLANATION...THIS IS JUST A PRACTICE EXERCISE FOR OUR UPCOMING ORAL AND THESE ARE THE SAMPLE QUESTIONS..PLEASE ANSWER SHORTER.. I WILL GIVE HELPFUL RATING AFTER

The spectroscopic data in the table is generated with five solutions of known concentration. Concentration (M) 0.0133 m= 0.0266 0.0532 0.106 0.213 Absorbance 0.1271 What is the intercept of the linear regression line? 0.08531 0.5388 1.069 Use a spreadsheet program, such as Microsoft Excel, to graph the data points and determine the equation of the best-fit line. 1.954 What is the slope of the linear regression line formed by these points? M-1

Pp

Rx tn.Oz /DMF what is the me Canissum 2

You prepare several dilutions of an unknown compound. You measure the absorbance of each solution at 340 nm using a 1 cm cuvette (your results are listed in the table below). What is the extinction coefficient (in (Mecm) ') of the compound? (Hint: assume that each of the individual values contains some degree of experimental error.) Concentration(uM) Absorbance at 340 nm 10.0 0.011 20.0 0.023 40.0 0.066 80.0 0.119 160.0 0.189

Calculate the cfu per ml of each dilutions and cfu per ml of the stock suspension (highlighted below). Show your solutions.

24

19. What is thin layer chromatography (TLC) LEAST useful for from the list below? A) To determine if crystallization or distillation may be more effective for a separation B) To determine the number of components in a mixture C) To determine the appropriate solvent for column- chromatographic separation D) To monitor the progress of an organic synthesis reaction 14. The solubility of salicylic acid in water is 7.8g/100ml at 100°C and 0.25g/100ml at 25°. Estimate how much water is needed to recrystallize a 19g sample of salicylic acid? A) 150ml B) 250ml C) 300ml D) 400ml