The synthesis of 3 − methylnon − 4 − yn − 3 − ol , using acetylene and compounds containing no more than four carbon atoms as starting material. Interpretation: The synthesis of 3 − methylnon − 4 − yn − 3 − ol , using acetylene and compounds containing no more than four carbon atoms as starting material is to be developed. Concept introduction: The synthesis of compound relies upon the type of reactants and reagents that are used during the reactions. The mechanism in alkenes and alkynes proceed through the breaking of double or triple bonds because pi bonds are less stable as compared to sigma bonds. The Stability of a product is the major factor that is responsible for the high yield of the product. The reagents perform numerous functions in reactions like proton abstraction, oxidation, reduction, catalysis, and dehydrogenation.

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Answer 1

Question

Chapter 9.10B, Problem 9.25P

(a)

Interpretation Introduction

To determine: The synthesis of 3−methylnon−4−yn−3−ol, using acetylene and compounds containing no more than four carbon atoms as starting material.

Interpretation: The synthesis of 3−methylnon−4−yn−3−ol, using acetylene and compounds containing no more than four carbon atoms as starting material is to be developed.

Concept introduction: The synthesis of compound relies upon the type of reactants and reagents that are used during the reactions. The mechanism in alkenes and alkynes proceed through the breaking of double or triple bonds because pi bonds are less stable as compared to sigma bonds.

The Stability of a product is the major factor that is responsible for the high yield of the product. The reagents perform numerous functions in reactions like proton abstraction, oxidation, reduction, catalysis, and dehydrogenation.

(b)

Interpretation Introduction

To determine: The synthesis of cis−1−ethyl−2−methylcyclopropane, using acetylene and compounds containing no more than four carbon atoms as starting material.

Interpretation: The synthesis of cis−1−ethyl−2−methylcyclopropane, using acetylene and compounds containing no more than four carbon atoms as starting material is to be developed.

Concept introduction: The synthesis of compound relies upon the type of reactants and reagents that are used during the reactions. The mechanism in alkene and alkynes proceed through the breaking of double or triple bonds because pi bonds are less stable.

The Stability of a product is the major factor that is responsible for the high yield of the product. The reagents perform numerous functions in reactions like proton abstraction, oxidation, reduction, catalysis, and dehydrogenation.

(c)

Interpretation Introduction

To determine: The synthesis of given compound, using acetylene and compounds containing no more than four carbon atoms as starting material.

Interpretation: The synthesis of given compound, using acetylene and compounds containing no more than four carbon atoms as starting material is to be developed.

Concept introduction: The synthesis of compound relies upon the type of reactants and reagents that are used during the reactions. The mechanism in alkene and alkynes proceed through the breaking of double or triple bonds because pi bonds are less stable.

The Stability of a product is the major factor that is responsible for the high yield of the product. The reagents perform numerous functions in reactions like proton abstraction, oxidation, reduction, catalysis, and dehydrogenation.

(d)

Interpretation Introduction

To determine: The synthesis of meso−hexane−3,4−diol, using acetylene and compounds containing no more than four carbon atoms as starting material.

Interpretation: The synthesis of meso−hexane−3,4−diol, using acetylene and compounds containing no more than four carbon atoms as starting material is to be developed.

Concept introduction: The synthesis of compound relies upon the type of reactants and reagents that are used during the reactions. The mechanism in alkene and alkynes proceed through the breaking of double or triple bonds because pi bonds are less stable.

The Stability of a product is the major factor that is responsible for the high yield of the product. The reagents perform numerous functions in reactions like proton abstraction, oxidation, reduction, catalysis, and dehydrogenation.

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(a 4 shows scanning electron microscope (SEM) images of extruded actions of packing bed for two capillary columns of different diameters, al 750 (bottom image) and b) 30-μm-i.d. Both columns are packed with the same stationary phase, spherical particles with 1-um diameter. A) When the columns were prepared, the figure shows that the column with the larger diameter has more packing irregularities. Explain this observation. B) Predict what affect this should have on band broadening and discuss your prediction using the van Deemter terms. C) Does this figure support your explanations in application question 33? Explain why or why not and make any changes in your answers in light of this figure. Figure 4 SEM images of sections of packed columns for a) 750 and b) 30-um-i.d. capillary columns.³

fcrip = ↓ bandwidth Il temp 32. What impact (increase, decrease, or no change) does each of the following conditions have on the individual components of the van Deemter equation and consequently, band broadening? Increase temperature Longer column Using a gas mobile phase instead of liquid Smaller particle stationary phase Multiple Paths Diffusion Mass Transfer

34. Figure 3 shows Van Deemter plots for a solute molecule using different column inner diameters (i.d.). A) Predict whether decreasing the column inner diameters increase or decrease bandwidth. B) Predict which van Deemter equation coefficient (A, B, or C) has the greatest effect on increasing or decreasing bandwidth as a function of i.d. and justify your answer. Figure 3 Van Deemter plots for hydroquinone using different column inner diameters (i.d. in μm). The data was obtained from liquid chromatography experiments using fused-silica capillary columns packed with 1.0-μm particles. 35 20 H(um) 큰 20 15 90 0+ 1500 100 75 550 01 02 594 05 μ(cm/sec) 30 15 10

Answer 2

Question

Chapter 9.10B, Problem 9.25P

(a)

Interpretation Introduction

To determine: The synthesis of 3−methylnon−4−yn−3−ol, using acetylene and compounds containing no more than four carbon atoms as starting material.

Interpretation: The synthesis of 3−methylnon−4−yn−3−ol, using acetylene and compounds containing no more than four carbon atoms as starting material is to be developed.

Concept introduction: The synthesis of compound relies upon the type of reactants and reagents that are used during the reactions. The mechanism in alkenes and alkynes proceed through the breaking of double or triple bonds because pi bonds are less stable as compared to sigma bonds.

The Stability of a product is the major factor that is responsible for the high yield of the product. The reagents perform numerous functions in reactions like proton abstraction, oxidation, reduction, catalysis, and dehydrogenation.

(b)

Interpretation Introduction

To determine: The synthesis of cis−1−ethyl−2−methylcyclopropane, using acetylene and compounds containing no more than four carbon atoms as starting material.

Interpretation: The synthesis of cis−1−ethyl−2−methylcyclopropane, using acetylene and compounds containing no more than four carbon atoms as starting material is to be developed.

Concept introduction: The synthesis of compound relies upon the type of reactants and reagents that are used during the reactions. The mechanism in alkene and alkynes proceed through the breaking of double or triple bonds because pi bonds are less stable.

The Stability of a product is the major factor that is responsible for the high yield of the product. The reagents perform numerous functions in reactions like proton abstraction, oxidation, reduction, catalysis, and dehydrogenation.

(c)

Interpretation Introduction

To determine: The synthesis of given compound, using acetylene and compounds containing no more than four carbon atoms as starting material.

Interpretation: The synthesis of given compound, using acetylene and compounds containing no more than four carbon atoms as starting material is to be developed.

Concept introduction: The synthesis of compound relies upon the type of reactants and reagents that are used during the reactions. The mechanism in alkene and alkynes proceed through the breaking of double or triple bonds because pi bonds are less stable.

The Stability of a product is the major factor that is responsible for the high yield of the product. The reagents perform numerous functions in reactions like proton abstraction, oxidation, reduction, catalysis, and dehydrogenation.

(d)

Interpretation Introduction

To determine: The synthesis of meso−hexane−3,4−diol, using acetylene and compounds containing no more than four carbon atoms as starting material.

Interpretation: The synthesis of meso−hexane−3,4−diol, using acetylene and compounds containing no more than four carbon atoms as starting material is to be developed.

Concept introduction: The synthesis of compound relies upon the type of reactants and reagents that are used during the reactions. The mechanism in alkene and alkynes proceed through the breaking of double or triple bonds because pi bonds are less stable.

The Stability of a product is the major factor that is responsible for the high yield of the product. The reagents perform numerous functions in reactions like proton abstraction, oxidation, reduction, catalysis, and dehydrogenation.

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Answer 3

Question

Chapter 9.10B, Problem 9.25P

(a)

Interpretation Introduction

To determine: The synthesis of 3−methylnon−4−yn−3−ol, using acetylene and compounds containing no more than four carbon atoms as starting material.

Interpretation: The synthesis of 3−methylnon−4−yn−3−ol, using acetylene and compounds containing no more than four carbon atoms as starting material is to be developed.

Concept introduction: The synthesis of compound relies upon the type of reactants and reagents that are used during the reactions. The mechanism in alkenes and alkynes proceed through the breaking of double or triple bonds because pi bonds are less stable as compared to sigma bonds.

The Stability of a product is the major factor that is responsible for the high yield of the product. The reagents perform numerous functions in reactions like proton abstraction, oxidation, reduction, catalysis, and dehydrogenation.

(b)

Interpretation Introduction

To determine: The synthesis of cis−1−ethyl−2−methylcyclopropane, using acetylene and compounds containing no more than four carbon atoms as starting material.

Interpretation: The synthesis of cis−1−ethyl−2−methylcyclopropane, using acetylene and compounds containing no more than four carbon atoms as starting material is to be developed.

Concept introduction: The synthesis of compound relies upon the type of reactants and reagents that are used during the reactions. The mechanism in alkene and alkynes proceed through the breaking of double or triple bonds because pi bonds are less stable.

The Stability of a product is the major factor that is responsible for the high yield of the product. The reagents perform numerous functions in reactions like proton abstraction, oxidation, reduction, catalysis, and dehydrogenation.

(c)

Interpretation Introduction

To determine: The synthesis of given compound, using acetylene and compounds containing no more than four carbon atoms as starting material.

Interpretation: The synthesis of given compound, using acetylene and compounds containing no more than four carbon atoms as starting material is to be developed.

Concept introduction: The synthesis of compound relies upon the type of reactants and reagents that are used during the reactions. The mechanism in alkene and alkynes proceed through the breaking of double or triple bonds because pi bonds are less stable.

The Stability of a product is the major factor that is responsible for the high yield of the product. The reagents perform numerous functions in reactions like proton abstraction, oxidation, reduction, catalysis, and dehydrogenation.

(d)

Interpretation Introduction

To determine: The synthesis of meso−hexane−3,4−diol, using acetylene and compounds containing no more than four carbon atoms as starting material.

Interpretation: The synthesis of meso−hexane−3,4−diol, using acetylene and compounds containing no more than four carbon atoms as starting material is to be developed.

Concept introduction: The synthesis of compound relies upon the type of reactants and reagents that are used during the reactions. The mechanism in alkene and alkynes proceed through the breaking of double or triple bonds because pi bonds are less stable.

The Stability of a product is the major factor that is responsible for the high yield of the product. The reagents perform numerous functions in reactions like proton abstraction, oxidation, reduction, catalysis, and dehydrogenation.

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Answer 4

Question

Chapter 9.10B, Problem 9.25P

(a)

Interpretation Introduction

To determine: The synthesis of 3−methylnon−4−yn−3−ol, using acetylene and compounds containing no more than four carbon atoms as starting material.

Interpretation: The synthesis of 3−methylnon−4−yn−3−ol, using acetylene and compounds containing no more than four carbon atoms as starting material is to be developed.

Concept introduction: The synthesis of compound relies upon the type of reactants and reagents that are used during the reactions. The mechanism in alkenes and alkynes proceed through the breaking of double or triple bonds because pi bonds are less stable as compared to sigma bonds.

The Stability of a product is the major factor that is responsible for the high yield of the product. The reagents perform numerous functions in reactions like proton abstraction, oxidation, reduction, catalysis, and dehydrogenation.

(b)

Interpretation Introduction

To determine: The synthesis of cis−1−ethyl−2−methylcyclopropane, using acetylene and compounds containing no more than four carbon atoms as starting material.

Interpretation: The synthesis of cis−1−ethyl−2−methylcyclopropane, using acetylene and compounds containing no more than four carbon atoms as starting material is to be developed.

Concept introduction: The synthesis of compound relies upon the type of reactants and reagents that are used during the reactions. The mechanism in alkene and alkynes proceed through the breaking of double or triple bonds because pi bonds are less stable.

The Stability of a product is the major factor that is responsible for the high yield of the product. The reagents perform numerous functions in reactions like proton abstraction, oxidation, reduction, catalysis, and dehydrogenation.

(c)

Interpretation Introduction

To determine: The synthesis of given compound, using acetylene and compounds containing no more than four carbon atoms as starting material.

Interpretation: The synthesis of given compound, using acetylene and compounds containing no more than four carbon atoms as starting material is to be developed.

Concept introduction: The synthesis of compound relies upon the type of reactants and reagents that are used during the reactions. The mechanism in alkene and alkynes proceed through the breaking of double or triple bonds because pi bonds are less stable.

The Stability of a product is the major factor that is responsible for the high yield of the product. The reagents perform numerous functions in reactions like proton abstraction, oxidation, reduction, catalysis, and dehydrogenation.

(d)

Interpretation Introduction

To determine: The synthesis of meso−hexane−3,4−diol, using acetylene and compounds containing no more than four carbon atoms as starting material.

Interpretation: The synthesis of meso−hexane−3,4−diol, using acetylene and compounds containing no more than four carbon atoms as starting material is to be developed.

Concept introduction: The synthesis of compound relies upon the type of reactants and reagents that are used during the reactions. The mechanism in alkene and alkynes proceed through the breaking of double or triple bonds because pi bonds are less stable.

The Stability of a product is the major factor that is responsible for the high yield of the product. The reagents perform numerous functions in reactions like proton abstraction, oxidation, reduction, catalysis, and dehydrogenation.

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Answer 5

Chapter 9.10B, Problem 9.25P

(a)

Interpretation Introduction

To determine: The synthesis of 3−methylnon−4−yn−3−ol, using acetylene and compounds containing no more than four carbon atoms as starting material.

Interpretation: The synthesis of 3−methylnon−4−yn−3−ol, using acetylene and compounds containing no more than four carbon atoms as starting material is to be developed.

Concept introduction: The synthesis of compound relies upon the type of reactants and reagents that are used during the reactions. The mechanism in alkenes and alkynes proceed through the breaking of double or triple bonds because pi bonds are less stable as compared to sigma bonds.

The Stability of a product is the major factor that is responsible for the high yield of the product. The reagents perform numerous functions in reactions like proton abstraction, oxidation, reduction, catalysis, and dehydrogenation.

(b)

Interpretation Introduction

To determine: The synthesis of cis−1−ethyl−2−methylcyclopropane, using acetylene and compounds containing no more than four carbon atoms as starting material.

Interpretation: The synthesis of cis−1−ethyl−2−methylcyclopropane, using acetylene and compounds containing no more than four carbon atoms as starting material is to be developed.

Concept introduction: The synthesis of compound relies upon the type of reactants and reagents that are used during the reactions. The mechanism in alkene and alkynes proceed through the breaking of double or triple bonds because pi bonds are less stable.

The Stability of a product is the major factor that is responsible for the high yield of the product. The reagents perform numerous functions in reactions like proton abstraction, oxidation, reduction, catalysis, and dehydrogenation.

(c)

Interpretation Introduction

To determine: The synthesis of given compound, using acetylene and compounds containing no more than four carbon atoms as starting material.

Interpretation: The synthesis of given compound, using acetylene and compounds containing no more than four carbon atoms as starting material is to be developed.

Concept introduction: The synthesis of compound relies upon the type of reactants and reagents that are used during the reactions. The mechanism in alkene and alkynes proceed through the breaking of double or triple bonds because pi bonds are less stable.

The Stability of a product is the major factor that is responsible for the high yield of the product. The reagents perform numerous functions in reactions like proton abstraction, oxidation, reduction, catalysis, and dehydrogenation.

(d)

Interpretation Introduction

To determine: The synthesis of meso−hexane−3,4−diol, using acetylene and compounds containing no more than four carbon atoms as starting material.

Interpretation: The synthesis of meso−hexane−3,4−diol, using acetylene and compounds containing no more than four carbon atoms as starting material is to be developed.

Concept introduction: The synthesis of compound relies upon the type of reactants and reagents that are used during the reactions. The mechanism in alkene and alkynes proceed through the breaking of double or triple bonds because pi bonds are less stable.

The Stability of a product is the major factor that is responsible for the high yield of the product. The reagents perform numerous functions in reactions like proton abstraction, oxidation, reduction, catalysis, and dehydrogenation.

Answer 6

Chapter 9.10B, Problem 9.25P

(a)

Interpretation Introduction

To determine: The synthesis of 3−methylnon−4−yn−3−ol, using acetylene and compounds containing no more than four carbon atoms as starting material.

Interpretation: The synthesis of 3−methylnon−4−yn−3−ol, using acetylene and compounds containing no more than four carbon atoms as starting material is to be developed.

Concept introduction: The synthesis of compound relies upon the type of reactants and reagents that are used during the reactions. The mechanism in alkenes and alkynes proceed through the breaking of double or triple bonds because pi bonds are less stable as compared to sigma bonds.

The Stability of a product is the major factor that is responsible for the high yield of the product. The reagents perform numerous functions in reactions like proton abstraction, oxidation, reduction, catalysis, and dehydrogenation.

Answer 7

Chapter 9.10B, Problem 9.25P

(a)

Interpretation Introduction

To determine: The synthesis of 3−methylnon−4−yn−3−ol, using acetylene and compounds containing no more than four carbon atoms as starting material.

Interpretation: The synthesis of 3−methylnon−4−yn−3−ol, using acetylene and compounds containing no more than four carbon atoms as starting material is to be developed.

Concept introduction: The synthesis of compound relies upon the type of reactants and reagents that are used during the reactions. The mechanism in alkenes and alkynes proceed through the breaking of double or triple bonds because pi bonds are less stable as compared to sigma bonds.

The Stability of a product is the major factor that is responsible for the high yield of the product. The reagents perform numerous functions in reactions like proton abstraction, oxidation, reduction, catalysis, and dehydrogenation.

Answer 8

(b)

Interpretation Introduction

To determine: The synthesis of cis−1−ethyl−2−methylcyclopropane, using acetylene and compounds containing no more than four carbon atoms as starting material.

Interpretation: The synthesis of cis−1−ethyl−2−methylcyclopropane, using acetylene and compounds containing no more than four carbon atoms as starting material is to be developed.

Concept introduction: The synthesis of compound relies upon the type of reactants and reagents that are used during the reactions. The mechanism in alkene and alkynes proceed through the breaking of double or triple bonds because pi bonds are less stable.

The Stability of a product is the major factor that is responsible for the high yield of the product. The reagents perform numerous functions in reactions like proton abstraction, oxidation, reduction, catalysis, and dehydrogenation.

Answer 9

(b)

Interpretation Introduction

To determine: The synthesis of cis−1−ethyl−2−methylcyclopropane, using acetylene and compounds containing no more than four carbon atoms as starting material.

Interpretation: The synthesis of cis−1−ethyl−2−methylcyclopropane, using acetylene and compounds containing no more than four carbon atoms as starting material is to be developed.

Concept introduction: The synthesis of compound relies upon the type of reactants and reagents that are used during the reactions. The mechanism in alkene and alkynes proceed through the breaking of double or triple bonds because pi bonds are less stable.

The Stability of a product is the major factor that is responsible for the high yield of the product. The reagents perform numerous functions in reactions like proton abstraction, oxidation, reduction, catalysis, and dehydrogenation.

Answer 10

(c)

Interpretation Introduction

To determine: The synthesis of given compound, using acetylene and compounds containing no more than four carbon atoms as starting material.

Interpretation: The synthesis of given compound, using acetylene and compounds containing no more than four carbon atoms as starting material is to be developed.

Concept introduction: The synthesis of compound relies upon the type of reactants and reagents that are used during the reactions. The mechanism in alkene and alkynes proceed through the breaking of double or triple bonds because pi bonds are less stable.

The Stability of a product is the major factor that is responsible for the high yield of the product. The reagents perform numerous functions in reactions like proton abstraction, oxidation, reduction, catalysis, and dehydrogenation.

Answer 11

(c)

Interpretation Introduction

To determine: The synthesis of given compound, using acetylene and compounds containing no more than four carbon atoms as starting material.

Interpretation: The synthesis of given compound, using acetylene and compounds containing no more than four carbon atoms as starting material is to be developed.

Concept introduction: The synthesis of compound relies upon the type of reactants and reagents that are used during the reactions. The mechanism in alkene and alkynes proceed through the breaking of double or triple bonds because pi bonds are less stable.

The Stability of a product is the major factor that is responsible for the high yield of the product. The reagents perform numerous functions in reactions like proton abstraction, oxidation, reduction, catalysis, and dehydrogenation.

Answer 12

(d)

Interpretation Introduction

To determine: The synthesis of meso−hexane−3,4−diol, using acetylene and compounds containing no more than four carbon atoms as starting material.

Interpretation: The synthesis of meso−hexane−3,4−diol, using acetylene and compounds containing no more than four carbon atoms as starting material is to be developed.

Concept introduction: The synthesis of compound relies upon the type of reactants and reagents that are used during the reactions. The mechanism in alkene and alkynes proceed through the breaking of double or triple bonds because pi bonds are less stable.

The Stability of a product is the major factor that is responsible for the high yield of the product. The reagents perform numerous functions in reactions like proton abstraction, oxidation, reduction, catalysis, and dehydrogenation.

Answer 13

(d)

Interpretation Introduction

To determine: The synthesis of meso−hexane−3,4−diol, using acetylene and compounds containing no more than four carbon atoms as starting material.

Interpretation: The synthesis of meso−hexane−3,4−diol, using acetylene and compounds containing no more than four carbon atoms as starting material is to be developed.

Concept introduction: The synthesis of compound relies upon the type of reactants and reagents that are used during the reactions. The mechanism in alkene and alkynes proceed through the breaking of double or triple bonds because pi bonds are less stable.

The Stability of a product is the major factor that is responsible for the high yield of the product. The reagents perform numerous functions in reactions like proton abstraction, oxidation, reduction, catalysis, and dehydrogenation.

Answer 14

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Answer 15

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Answer 16

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Answer 17

Ch. 9.1 - a. Count the elements of unsaturation in...Ch. 9.2 - Prob. 9.2P Ch. 9.4B - What reaction would acetylene likely undergo if it...Ch. 9.6 - Prob. 9.4P Ch. 9.6 - Predict the products of the following acid-base...Ch. 9.7A - Solved Problem9-1 showed the synthesis of...Ch. 9.7A - Show how you might synthesize the following...Ch. 9.7B - Prob. 9.8P Ch. 9.7B - Show how you would synthesize...Ch. 9.8 - When 2,2-dibromo-1-phenylpropane is heated...

Solution Summary: The author explains how the synthesis of compounds depends upon the type of reactants and reagents that are used during the reactions. Stability of a product is responsible for the high yield of the product.

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