Chemistry
4th Edition
ISBN: 9780393919370
Author: Thomas R. Gilbert
Publisher: NORTON
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Chapter 3, Problem 3.105QP
Interpretation Introduction
Interpretation: The reasons corresponding to the actual yield from a
Concept introduction: The actual yield is the experimentally observed yield but the theoretical yield is the calculated yield.
To determine: If the percent yield of a chemical reaction can exceed
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Assign this HSQC Spectrum ( please editing clearly on the image)
(a
4 shows scanning electron microscope (SEM) images of extruded
actions of packing bed for two capillary columns of different diameters,
al 750 (bottom image) and b) 30-μm-i.d. Both columns are packed with the
same stationary phase, spherical particles with 1-um diameter.
A) When the columns were prepared, the figure shows that the column with
the larger diameter has more packing irregularities. Explain this observation.
B) Predict what affect this should have on band broadening and discuss your
prediction using the van Deemter terms.
C) Does this figure support your explanations in application question 33?
Explain why or why not and make any changes in your answers in light of
this figure.
Figure 4 SEM images of
sections of packed columns
for a) 750 and b) 30-um-i.d.
capillary columns.³
fcrip
= ↓ bandwidth Il temp
32. What impact (increase, decrease, or no change) does each of the following conditions have on the individual
components of the van Deemter equation and consequently, band broadening?
Increase temperature
Longer column
Using a gas mobile phase
instead of liquid
Smaller particle stationary phase
Multiple Paths
Diffusion
Mass Transfer
Chapter 3 Solutions
Chemistry
Ch. 3.2 - Prob. 1PECh. 3.2 - Prob. 2PECh. 3.2 - Prob. 3PECh. 3.2 - Prob. 4PECh. 3.2 - Prob. 5PECh. 3.2 - Prob. 6PECh. 3.2 - Prob. 8PECh. 3.3 - Prob. 9PECh. 3.3 - Prob. 10PECh. 3.4 - Prob. 11PE
Ch. 3.5 - Prob. 12PECh. 3.5 - Prob. 13PECh. 3.6 - Prob. 14PECh. 3.6 - Prob. 16PECh. 3.7 - Prob. 17PECh. 3.8 - Prob. 18PECh. 3.8 - Prob. 19PECh. 3.9 - Prob. 20PECh. 3.9 - Prob. 21PECh. 3.9 - Prob. 22PECh. 3.9 - Prob. 23PECh. 3 - Prob. 3.1VPCh. 3 - Prob. 3.2VPCh. 3 - Prob. 3.3VPCh. 3 - Prob. 3.4VPCh. 3 - Prob. 3.5VPCh. 3 - Prob. 3.6VPCh. 3 - Prob. 3.7VPCh. 3 - Prob. 3.8VPCh. 3 - Prob. 3.9QPCh. 3 - Prob. 3.10QPCh. 3 - Prob. 3.11QPCh. 3 - Prob. 3.12QPCh. 3 - Prob. 3.13QPCh. 3 - Prob. 3.14QPCh. 3 - Prob. 3.15QPCh. 3 - Prob. 3.16QPCh. 3 - Prob. 3.17QPCh. 3 - Prob. 3.18QPCh. 3 - Prob. 3.19QPCh. 3 - Prob. 3.20QPCh. 3 - Prob. 3.21QPCh. 3 - Prob. 3.22QPCh. 3 - Prob. 3.23QPCh. 3 - Prob. 3.24QPCh. 3 - Prob. 3.25QPCh. 3 - Prob. 3.26QPCh. 3 - Prob. 3.27QPCh. 3 - Prob. 3.28QPCh. 3 - Prob. 3.29QPCh. 3 - Prob. 3.30QPCh. 3 - Prob. 3.31QPCh. 3 - Prob. 3.32QPCh. 3 - Prob. 3.33QPCh. 3 - Prob. 3.34QPCh. 3 - Prob. 3.35QPCh. 3 - Prob. 3.36QPCh. 3 - Prob. 3.37QPCh. 3 - Prob. 3.38QPCh. 3 - Prob. 3.39QPCh. 3 - Prob. 3.40QPCh. 3 - Prob. 3.41QPCh. 3 - Prob. 3.42QPCh. 3 - Prob. 3.43QPCh. 3 - Prob. 3.44QPCh. 3 - Prob. 3.45QPCh. 3 - Prob. 3.46QPCh. 3 - Prob. 3.47QPCh. 3 - Prob. 3.48QPCh. 3 - Prob. 3.49QPCh. 3 - Prob. 3.50QPCh. 3 - Prob. 3.51QPCh. 3 - Prob. 3.52QPCh. 3 - Prob. 3.53QPCh. 3 - Prob. 3.54QPCh. 3 - Prob. 3.55QPCh. 3 - Prob. 3.56QPCh. 3 - Prob. 3.57QPCh. 3 - Prob. 3.58QPCh. 3 - Prob. 3.59QPCh. 3 - Prob. 3.60QPCh. 3 - Prob. 3.61QPCh. 3 - Prob. 3.62QPCh. 3 - Prob. 3.63QPCh. 3 - Prob. 3.64QPCh. 3 - Prob. 3.65QPCh. 3 - Prob. 3.66QPCh. 3 - Prob. 3.67QPCh. 3 - Prob. 3.68QPCh. 3 - Prob. 3.69QPCh. 3 - Prob. 3.70QPCh. 3 - Prob. 3.71QPCh. 3 - Prob. 3.72QPCh. 3 - Prob. 3.73QPCh. 3 - Prob. 3.74QPCh. 3 - Prob. 3.75QPCh. 3 - Prob. 3.76QPCh. 3 - Prob. 3.77QPCh. 3 - Prob. 3.78QPCh. 3 - Prob. 3.79QPCh. 3 - Prob. 3.80QPCh. 3 - Prob. 3.81QPCh. 3 - Prob. 3.82QPCh. 3 - Prob. 3.83QPCh. 3 - Prob. 3.84QPCh. 3 - Prob. 3.85QPCh. 3 - Prob. 3.86QPCh. 3 - Prob. 3.87QPCh. 3 - Prob. 3.88QPCh. 3 - Prob. 3.89QPCh. 3 - Prob. 3.90QPCh. 3 - Prob. 3.91QPCh. 3 - Prob. 3.92QPCh. 3 - Prob. 3.93QPCh. 3 - Prob. 3.94QPCh. 3 - Prob. 3.95QPCh. 3 - Prob. 3.96QPCh. 3 - Prob. 3.97QPCh. 3 - Prob. 3.98QPCh. 3 - Prob. 3.99QPCh. 3 - Prob. 3.100QPCh. 3 - Prob. 3.101QPCh. 3 - Prob. 3.102QPCh. 3 - Prob. 3.103QPCh. 3 - Prob. 3.104QPCh. 3 - Prob. 3.105QPCh. 3 - Prob. 3.106QPCh. 3 - Prob. 3.107QPCh. 3 - Prob. 3.108QPCh. 3 - Prob. 3.109QPCh. 3 - Prob. 3.110QPCh. 3 - Prob. 3.111QPCh. 3 - Prob. 3.112QPCh. 3 - Prob. 3.113QPCh. 3 - Prob. 3.114QPCh. 3 - Prob. 3.115QPCh. 3 - Prob. 3.116QPCh. 3 - Prob. 3.117APCh. 3 - Prob. 3.118APCh. 3 - Prob. 3.119APCh. 3 - Prob. 3.120APCh. 3 - Prob. 3.121APCh. 3 - Prob. 3.122APCh. 3 - Prob. 3.123APCh. 3 - Prob. 3.124APCh. 3 - Prob. 3.125APCh. 3 - Prob. 3.126APCh. 3 - Prob. 3.127APCh. 3 - Prob. 3.128APCh. 3 - Prob. 3.129APCh. 3 - Prob. 3.130APCh. 3 - Prob. 3.131APCh. 3 - Prob. 3.132APCh. 3 - Prob. 3.133APCh. 3 - Prob. 3.134APCh. 3 - Prob. 3.135APCh. 3 - Prob. 3.136APCh. 3 - Prob. 3.137APCh. 3 - Prob. 3.138APCh. 3 - Prob. 3.139APCh. 3 - Prob. 3.140APCh. 3 - Prob. 3.141APCh. 3 - Prob. 3.142APCh. 3 - Prob. 3.143APCh. 3 - Prob. 3.144AP
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