1 Introduction 2 Laboratory Safety, Courtesy, And Waste Disposal 3 Melting Points And Boiling Points 4 Recrystallization 5 Distillation 6 Steam Distillation, Vacuum Distillation, And Sublimation 7 Extraction 8 Thin-layer Chromatography: Analyzing Analgesics And Isolating Lycopene From Tomato Paste 9 Column Chromatography: Fluorenone, Cholesteryl Acetate, Acetylferrocene, And Plant Pigments 10 Gas Chromatography: Analyzing Alkene Isomers 11 Infrared Spectroscopy 12 Nuclear Magnetic Resonance Spectroscopy 13 Mass Spectrometry 14 Ultraviolet Spectroscopy, Refractive Indices, And Qualitative Instrumental Organic Analysis 15 Computational Chemistry 16 The Sn2 Reaction: 1-bromobutane 17 Nucleophilic Substitution Reactions Of Alkyl Halides 18 Radical Initiated Chlorination Of 1-chlorobutane 19 Alkenes From Alcohols: Cyclohexene From Cyclohexanol 20 Bromination And Debromination: Purification Of Cholesterol 21 Dichlorocarbene 22 Oxidation: Cyclohexanol To Cyclohexanone; Cyclohexanone To Adipic Acid 23 The Cannizzaro Reaction: Simultaneous Synthesis Of An Alcohol And An Acid In The Absence Of 24 Oxidative Coupling Of Alkynes: 2,7-dimethyl-3,5-octadiyn-2,7-diol 25 Catalytic Hydrogenation 26 Sodium Borohydride Reduction Of 2-methylcyclohexanone: A Problem In Conformational 27 Epoxidation Of Cholesterol 28 Nitration Of Methyl Benzoate 29 Friedel-crafts Alkylation Of Benzene And Dimethoxybenzene; Host-guest Chemistry 30 Alkylation Of Mesitylene 31 The Friedel-crafts Reaction: Anthraquinone And Anthracene 32 Friedel-crafts Acylation Of Ferrocene: Acetylferrocene 33 Reactions Of Triphenylmethyl Carbocation, Carbanion, And Radical 34 1,2,3,4-tetraphenyl-naphthalene Via Benzyne 35 Triptycene Via Benzyne 36 Aldehydes And Ketones 37 Dibenzalacetone By The Aldol Condensation 38 Grignard Synthesis Of Triphenylmethanol And Benzoic Acid 39 The Wittig And Wittig-horner Reactions 40 Esterification And Hydrolysis 41 Acetylsalicylic Acid (aspirin) 42 Malonic Ester Of A Barbiturate 43 Amines 44 The Sandmeyer Reaction:1-bromo-4-chlorobenzene, 2-iodobenzoic Acid, And 4-chlorotoluene 45 Synthesis And Bioassay Of Sulfanilamide And Derivatives 46 Dyes And Dyeing 47 Martius Yellow 48 Diels-alder Reaction 49 Ferrocene [bis(cyclopentadienyl)iron] 50 A Diels-alder Reaction Puzzle: The Reaction Of 2,4-hexadien-1-ol With Maleic Anhydride 51 Tetraphenylcyclopentadienone 52 Hexaphenylbenzene And Dimethyl Tetraphenylphthalate 53 The Benzoin Condensation: Catalysis By The Cyanide Ion And Thiamine 54 Nitric Acid Oxidation; Preparation Of Benzil From Benzoin; And Synthesis Of A Heterocycle: Diphenylquinoxaline 55 The Borohydride Reduction Of A Ketone: Hydrobenzoin From Benzil 56 The Synthesis Of 2,2-dimethyl-1,5-dioxolane; The Acetonide Derivative Of A Vicinal Diol 57 1,4-addition: Reductive Acetylation Of Benzil 58 The Synthesis Of An Alkyne From An Alkene By Bromination And Dehydrobromination: Stilbene And Diphenylacetylene 59 The Perkin Reaction: Synthesis Of A-phenylcinnamic Acid And Its Decarboxylation To Cis-stilbene 60 Multicomponent Reactions: The Aqueous Passerini Reaction 61 Chemiluminescence: Syntheses Of Cyalume And Luminol 62 Photochemistry: The Synthesis Of Benzopinacol 63 Carbohydrates And Sweeteners 64 Virstatin, A Possible Treatment For Cholera 65 Biosynthesis Of Ethanol And Enzymatic Reactions 66 The Synthesis Of Natural Products: The Sex Attractant Of The Cockroach And Camphor 67 polymers: Synthesis And Recycling 68 Searching The Chemical Literature expand_more
Principles of Instrumental AnalysisChemistryISBN:9781305577213Author:Douglas A. Skoog, F. James Holler, Stanley R. CrouchPublisher:Cengage Learning