The Organic Chem Lab Survival Manual: A Student's Guide to Techniques
The Organic Chem Lab Survival Manual: A Student's Guide to Techniques
10th Edition
ISBN: 9781118875780
Author: James W. Zubrick
Publisher: WILEY
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Chapter 10, Problem 2E
Interpretation Introduction

Interpretation: Anhydrous potassium carbonate is useful for drying amines whilenot acids, so much are to be explained.

Concept Introduction:

➢ A drying agent is a chemical used to remove water from an organic compound that is in solution. Potassium carbonate, phosphorous pentoxide, magnesium sulfate, or potassium chloride etc., are used as drying agent.

➢ Drying agents are usually certain anhydrous salts that combine with water in the product and hold it as water of crystallization.

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Part II. Given below are the 'H-NMR spectrum at 300 MHz in CDC13 and mass spectrum using electron ionization of compound Brian. The FTIR of the said compound showed a strong peak at 1710 cm"). Determine the following: (a) molecular Formula and Degree of unsaturation of compound Brian (b) Basing on the given H-NMR spectrum tabulate the following (i) chemical shifts (ii) integration, ciii) multiplicity and (iv) interferences made for each signal (c) Draw the structure of compound Brian. ) ΕΙ 43 41 27 71 114 (M+) Hmmm 20 30 40 50 60 70 80 90 100 110 120 1H NMR spectrum 300 MHz in CDCl3 2.0 alle 1.0

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The Organic Chem Lab Survival Manual: A Student's Guide to Techniques

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