You have an organic acid, organic base, and a neutral organic compound all together in a solid mixture. What steps would you take, in order, to isolate the organic acid? 1. 2. 3. 4. To the combined aqueous extracts, add 6M NaOH(aq) until the solution is basic. Dry the solution in the beaker with sodium sulfate, filter, and evaporate off the solvent. Filter to collect the solid. Add 3M HCI(aq) and shake and vent, then transfer aqeous phase to a separate flask. Repeat two times. Rinse the organic phase with brine and transfer to a beaker. Dissolve the crude solid in ether and place separatory funnel. Add 3M NaOH(aq) and shake and vent, then transfer aqeous phase to a separate beaker. Repeat two times To the combined aqueous extracts, add 6M HC\(aq) until the solution is acidic.

You have an organic acid, organic base, and a neutral organic compound all together in a solid mixture. What steps would you take, in order, to isolate the organic acid? 1. 2. 3. 4. To the combined aqueous extracts, add 6M NaOH(aq) until the solution is basic. Dry the solution in the beaker with sodium sulfate, filter, and evaporate off the solvent. Filter to collect the solid. Add 3M HCI(aq) and shake and vent, then transfer aqeous phase to a separate flask. Repeat two times. Rinse the organic phase with brine and transfer to a beaker. Dissolve the crude solid in ether and place separatory funnel. Add 3M NaOH(aq) and shake and vent, then transfer aqeous phase to a separate beaker. Repeat two times To the combined aqueous extracts, add 6M HC\(aq) until the solution is acidic.

Chemistry

10th Edition

ISBN:9781305957404

Author:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste

Publisher:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste

Chapter1: Chemical Foundations

Section: Chapter Questions

Problem 1RQ: Define and explain the differences between the following terms. a. law and theory b. theory and...

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