Use the binary diagram, 45 line above and material balance to solve the One thousand kg/h of a (50-50 wt%) acetone-in-water solution is to be extracted at 25C in a continuous, countercurrent system with pure 1,1,2-trichloroethane to obtain a raffinate containing 10 wt% acetone. Using the following equilibrium data, determine with an equilateral-triangle diagram: a the minimum flow rate of solvent; b. the number of stages required for a solvent rate equal to 1.5 times minimum, and composition of each streamleaving each stage. Repeat the calculation of (a) and (b) if the solvent used has purity 93wt% (4wr% acetone, 3wt% water impurities) acetone 0.6 water 0.13 1,1,2-trichloroethane 0.27 Raffinate. Weight Fraction Acetone Extract. Weight Fraction Acetone 0.5 0.04 0.46 0.44 0.56 0.4 0.03 0.57 0.29 0.40 0.3 0.02 0.681 0.12 0.18 0.2 0.015 0.785 0.0 0.0 0.1 0.01 0.89 0.55 0.35 0.1 0.5 0.43 0.07 0.4 0.57 0.03 0.3 0.68 0.02 0.2 0.79 0.01 0.1 0.895 0.005

Introduction to Chemical Engineering Thermodynamics
8th Edition
ISBN:9781259696527
Author:J.M. Smith Termodinamica en ingenieria quimica, Hendrick C Van Ness, Michael Abbott, Mark Swihart
Publisher:J.M. Smith Termodinamica en ingenieria quimica, Hendrick C Van Ness, Michael Abbott, Mark Swihart
Chapter1: Introduction
Section: Chapter Questions
Problem 1.1P
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Use the binary diagram, 45 line above and material balance to solve the
One thousand kg/h of a (50-50 wt%) acetone-in-water solution is to be extracted at 25C in a continuous,
countercurrent system with pure 1,1,2-trichloroethane to obtain a raffinate containing 10 wt% acetone. Using the
following equilibrium data, determine with an equilateral-triangle diagram:
a the minimum flow rate of solvent;
b. the number of stages required for a solvent rate equal to 1.5 times minimum, and composition of each
streamleaving each stage.
Repeat the calculation of (a) and (b) if the solvent used has purity 93wt% (4wr% acetone, 3wt% water
impurities)
acetone
0.6
water
0.13
1,1,2-trichloroethane
0.27
Raffinate. Weight
Fraction Acetone
Extract. Weight
Fraction Acetone
0.5
0.04
0.46
0.44
0.56
0.4
0.03
0.57
0.29
0.40
0.3
0.02
0.681
0.12
0.18
0.2
0.015
0.785
0.0
0.0
0.1
0.01
0.89
0.55
0.35
0.1
0.5
0.43
0.07
0.4
0.57
0.03
0.3
0.68
0.02
0.2
0.79
0.01
0.1
0.895
0.005
Transcribed Image Text:Use the binary diagram, 45 line above and material balance to solve the One thousand kg/h of a (50-50 wt%) acetone-in-water solution is to be extracted at 25C in a continuous, countercurrent system with pure 1,1,2-trichloroethane to obtain a raffinate containing 10 wt% acetone. Using the following equilibrium data, determine with an equilateral-triangle diagram: a the minimum flow rate of solvent; b. the number of stages required for a solvent rate equal to 1.5 times minimum, and composition of each streamleaving each stage. Repeat the calculation of (a) and (b) if the solvent used has purity 93wt% (4wr% acetone, 3wt% water impurities) acetone 0.6 water 0.13 1,1,2-trichloroethane 0.27 Raffinate. Weight Fraction Acetone Extract. Weight Fraction Acetone 0.5 0.04 0.46 0.44 0.56 0.4 0.03 0.57 0.29 0.40 0.3 0.02 0.681 0.12 0.18 0.2 0.015 0.785 0.0 0.0 0.1 0.01 0.89 0.55 0.35 0.1 0.5 0.43 0.07 0.4 0.57 0.03 0.3 0.68 0.02 0.2 0.79 0.01 0.1 0.895 0.005
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