Chemistry
10th Edition
ISBN:9781305957404
Author:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Publisher:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Chapter1: Chemical Foundations
Section: Chapter Questions
Problem 1RQ: Define and explain the differences between the following terms. a. law and theory b. theory and...
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Question
A solution containing orange rind extract was analyzed using gas chromatography to measure its limonene content. The parameters used to analyze the standards and samples are listed below. Calculate the concentration of limonene in the solution in ug/mL
Transcribed Image Text:Table 1. Operation Specifications for GC.
Gas Chromatograph: PerkinElmer Clarus 500 GC
Analytical Column:
Elite-Sms (30 m x 0.25 mm x 0.25 um)
Injector-Port Type:
Capillary
Injector-Port Temp:
250 'C
Injection Type:
Split (20 ml./min)
Syringe Volume:
5 uL
Injection Volume:
0.5 ul
Injection Speed:
Fast
Rinse Solvent:
Methanol
Carrier-Gas Program: 1 ml/min
Oven Program:
Temperature Hold Time Rate
80 'C
3 min
5 "C/min
140 'C
O min
45 'C/min
275 'C
Hold
Transcribed Image Text:Limonene, ug/mL Response
5
7024
10
11731
25
25852
50
49388
100
96458
Sample Solution
35850
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