synthesis of 2-Chloro-2-Methylbutane -Centrifuge cleared +10mL Centrifuge tube. -4ml 2-methyl-2-butanol added to Centrifuge tube. -5ml Hydrochloric added CT -Shaked for 3 min - Two Layers formed - aqueous layer pipetted out into the beaker set aside. - 2ml water added To CT, inverted vented few times. - aqueous layer pipet out to beaker - 2ml 5% sodium bicarbonate, added to CT, inverted and vent and aqueous layer pipet out into the beaker -Centrifuge Tube poured into a cleaned 5mL conical vial - a few scoops of soduim sulfate added to the CV and stirred well - new 5mL Conical vial with teflon stopper preweighted 25.90g - liquid decanted into the new conical vial - conical vial + liquid capped and weighted 26.40g CALCULATIONS: % YIELDS FOR the REACTION SHOW ALL WORK
Lab observation sheet
synthesis of 2-Chloro-2-Methylbutane
-Centrifuge cleared +10mL Centrifuge tube.
-4ml 2-methyl-2-butanol added to Centrifuge tube.
-5ml Hydrochloric added CT
-Shaked for 3 min
- Two Layers formed
- aqueous layer pipetted out into the beaker set aside.
- 2ml water added To CT, inverted vented few times.
- aqueous layer pipet out to beaker
- 2ml 5% sodium bicarbonate, added to CT, inverted and vent and aqueous layer pipet out into the beaker
-Centrifuge Tube poured into a cleaned 5mL conical vial
- a few scoops of soduim sulfate added to the CV and stirred well
- new 5mL Conical vial with teflon stopper preweighted 25.90g
- liquid decanted into the new conical vial
- conical vial + liquid capped and weighted 26.40g
CALCULATIONS:
% YIELDS FOR the REACTION SHOW ALL WORK
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