synthesis of 2-Chloro-2-Methylbutane -Centrifuge cleared +10mL Centrifuge tube. -4ml 2-methyl-2-butanol added to Centrifuge tube. -5ml Hydrochloric added CT -Shaked for 3 min - Two Layers formed - aqueous layer pipetted out into the beaker set aside. - 2ml water added To CT, inverted vented few times. - aqueous layer pipet out to beaker - 2ml 5% sodium bicarbonate, added to CT, inverted and vent and aqueous layer pipet out into the beaker -Centrifuge Tube poured into a cleaned 5mL conical vial - a few scoops of soduim sulfate added to the CV and stirred well - new 5mL Conical vial with teflon stopper preweighted 25.90g - liquid decanted into the new conical vial - conical vial + liquid capped and weighted 26.40g CALCULATIONS: % YIELDS FOR the REACTION SHOW ALL WORK

Chemistry
10th Edition
ISBN:9781305957404
Author:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Publisher:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Chapter1: Chemical Foundations
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Problem 1RQ: Define and explain the differences between the following terms. a. law and theory b. theory and...
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Lab observation sheet

synthesis of 2-Chloro-2-Methylbutane

-Centrifuge cleared +10mL Centrifuge tube.

-4ml 2-methyl-2-butanol added to Centrifuge tube.

-5ml Hydrochloric added CT

-Shaked for 3 min

- Two Layers formed

- aqueous layer pipetted out into the beaker set aside.

- 2ml water added To CT, inverted vented few times.

- aqueous layer pipet out to beaker

- 2ml 5% sodium bicarbonate, added to CT, inverted and vent and aqueous layer pipet out into the beaker

-Centrifuge Tube poured into a cleaned 5mL conical vial

- a few scoops of soduim sulfate added to the CV and stirred well

- new 5mL Conical vial with teflon stopper preweighted 25.90g

- liquid decanted into the new conical vial

- conical vial + liquid capped and weighted 26.40g

CALCULATIONS:

% YIELDS FOR the REACTION SHOW ALL WORK

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