Separations: You have carried out the below reaction between an acid chloride with an amine to form an amide. Construct a flow chart to show how you would isolate the product from unreacted starting materials using a reactive acid base extraction. Keep in mind that acid chlorides are readily hydrolyzed to carboxylic acids in the presence of aqueous acid or base, and that amides are not extracted into aqueous acid or base. Assume you have DCM, 1.0M HCl, 1.0M NaOH, and saturated NaHCO. CI + H₂N excess CH2Cl2
Separations: You have carried out the below reaction between an acid chloride with an amine to form an amide. Construct a flow chart to show how you would isolate the product from unreacted starting materials using a reactive acid base extraction. Keep in mind that acid chlorides are readily hydrolyzed to carboxylic acids in the presence of aqueous acid or base, and that amides are not extracted into aqueous acid or base. Assume you have DCM, 1.0M HCl, 1.0M NaOH, and saturated NaHCO. CI + H₂N excess CH2Cl2
Chemistry
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ISBN:9781305957404
Author:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
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Chapter1: Chemical Foundations
Section: Chapter Questions
Problem 1RQ: Define and explain the differences between the following terms. a. law and theory b. theory and...
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![Separations:
You have carried out the below reaction between an acid
chloride with an amine to form an amide. Construct a flow chart
to show how you would isolate the product from unreacted
starting materials using a reactive acid base extraction. Keep in
mind that acid chlorides are readily hydrolyzed to carboxylic
acids in the presence of aqueous acid or base, and that amides
are not extracted into aqueous acid or base. Assume you have
DCM, 1.0M HCl, 1.0M NaOH, and saturated NaHCO.
CI + H₂N
excess
CH2Cl2](/v2/_next/image?url=https%3A%2F%2Fcontent.bartleby.com%2Fqna-images%2Fquestion%2Fc2259ed3-0e09-44b7-8246-fefbeed72c9e%2F0264cfa5-eee3-42d3-914b-c36316f86578%2F14jeynq_processed.jpeg&w=3840&q=75)
Transcribed Image Text:Separations:
You have carried out the below reaction between an acid
chloride with an amine to form an amide. Construct a flow chart
to show how you would isolate the product from unreacted
starting materials using a reactive acid base extraction. Keep in
mind that acid chlorides are readily hydrolyzed to carboxylic
acids in the presence of aqueous acid or base, and that amides
are not extracted into aqueous acid or base. Assume you have
DCM, 1.0M HCl, 1.0M NaOH, and saturated NaHCO.
CI + H₂N
excess
CH2Cl2
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