QI Solid potassium sulfate (K2SO4) is obtained from an aqueous solution of this salt via two unit operations process, which are an evaporator and a unit of crystalizer and filter combination. The fresh feed to the process contains 19.6 wt% K2SO4. The evaporator has a maximum capacity to evaporate 175 kg water/s and can be able to evaporate 45.0% water of the feed. The wet filter cake discharged from the crystalizer-filter unit contains solid K;SO4 crystals and a 40.0 wt% K SO, solution, in a ratio 10 kg crystals/kg solution. The 40.0 wt% K:SO4 solution filtrate from crystalizer-filter unit is recycled to join the fresh feed.

Introduction to Chemical Engineering Thermodynamics
8th Edition
ISBN:9781259696527
Author:J.M. Smith Termodinamica en ingenieria quimica, Hendrick C Van Ness, Michael Abbott, Mark Swihart
Publisher:J.M. Smith Termodinamica en ingenieria quimica, Hendrick C Van Ness, Michael Abbott, Mark Swihart
Chapter1: Introduction
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Solid potassium sulfate (K2SO4) is obtained from an aqueous solution of this salt
via two unit operations process, which are an evaporator and a unit of crystalizer
and filter combination. The fresh feed to the process contains 19.6 wt% K2SO4. The
evaporator has a maximum capacity to evaporate 175 kg water/s and can be able to
evaporate 45.0% water of the feed. The wet filter cake discharged from the
crystalizer-filter unit contains solid K,SO4 crystals and a 40.0 wt% K,SO, solution,
in a ratio 10 kg crystals/kg solution. The 40.0 wt% K2SO4 solution filtrate from
crystalizer-filter unit is recycled to join the fresh feed.
(a)
Assume the process is operating at maximum capacity,
(i) Illustrate a completely labelled flowchart of this process.
(ii) Analyze the degree-of-freedom for the overall system, recycle-fresh feed
mixing point, evaporator, and crystalizer-filter unit.
(b)
Calculate the maximum production rate of solid K2SO4, the rate at which fresh feed
must be supplied to achieve this production rate, and the ratio kg recycle/kg fresh
feed.
Calculate the compositions and feed rate of the stream entering the crystallizer-
filter unit if the process is scaled to 75% of its maximum capacity.
(c)
Transcribed Image Text:QI Solid potassium sulfate (K2SO4) is obtained from an aqueous solution of this salt via two unit operations process, which are an evaporator and a unit of crystalizer and filter combination. The fresh feed to the process contains 19.6 wt% K2SO4. The evaporator has a maximum capacity to evaporate 175 kg water/s and can be able to evaporate 45.0% water of the feed. The wet filter cake discharged from the crystalizer-filter unit contains solid K,SO4 crystals and a 40.0 wt% K,SO, solution, in a ratio 10 kg crystals/kg solution. The 40.0 wt% K2SO4 solution filtrate from crystalizer-filter unit is recycled to join the fresh feed. (a) Assume the process is operating at maximum capacity, (i) Illustrate a completely labelled flowchart of this process. (ii) Analyze the degree-of-freedom for the overall system, recycle-fresh feed mixing point, evaporator, and crystalizer-filter unit. (b) Calculate the maximum production rate of solid K2SO4, the rate at which fresh feed must be supplied to achieve this production rate, and the ratio kg recycle/kg fresh feed. Calculate the compositions and feed rate of the stream entering the crystallizer- filter unit if the process is scaled to 75% of its maximum capacity. (c)
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