Provide separate answers to the following questions but also include them in your discussion section of the report a) Diethyl ether is a hazardous solvent since, as well as being highly flammable; it can form explosive peroxide - exercise caution and be safety conscious. The work-up in the standard scale experiment includes a step to remove any such peroxides. Which is this step? b) Why is a gas evolved during the carbonate extraction? What is it? c) Write a reaction mechanism for the esterification reaction between ethanoic acid and 3- methylbutan-1-ol. What is the role of the sulfuric acid? d) Examine the IR spectrum of 3-methyl butyl ethanoate provided. Assign the peaks which correspond to the C=O and C-O bonds in the molecule. e) Examine the NMR spectrum of 3-methylbutyl provided. Assign peaks to each of the groups of protons within the molecule.
Provide separate answers to the following questions but also include them in your discussion section of the report a) Diethyl ether is a hazardous solvent since, as well as being highly flammable; it can form explosive peroxide - exercise caution and be safety conscious. The work-up in the standard scale experiment includes a step to remove any such peroxides. Which is this step? b) Why is a gas evolved during the carbonate extraction? What is it? c) Write a reaction mechanism for the esterification reaction between ethanoic acid and 3- methylbutan-1-ol. What is the role of the sulfuric acid? d) Examine the IR spectrum of 3-methyl butyl ethanoate provided. Assign the peaks which correspond to the C=O and C-O bonds in the molecule. e) Examine the NMR spectrum of 3-methylbutyl provided. Assign peaks to each of the groups of protons within the molecule.
Chemistry
10th Edition
ISBN:9781305957404
Author:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Publisher:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Chapter1: Chemical Foundations
Section: Chapter Questions
Problem 1RQ: Define and explain the differences between the following terms. a. law and theory b. theory and...
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Answer these questions.
Transcribed Image Text:Provide separate answers to the following questions but also include them in your discussion
section of the report
a) Diethyl ether is a hazardous solvent since, as well as being highly flammable; it can form
explosive peroxide - exercise caution and be safety conscious. The work-up in the standard
scale experiment includes a step to remove any such peroxides. Which is this step?
b) Why is a gas evolved during the carbonate extraction? What is it?
c) Write a reaction mechanism for the esterification reaction between ethanoic acid and 3-
methylbutan-1-ol. What is the role of the sulfuric acid?
d) Examine the IR spectrum of 3-methyl butyl ethanoate provided. Assign the peaks which
correspond to the C=O and C-O bonds in the molecule.
e) Examine the NMR spectrum of 3-methylbutyl provided. Assign peaks to each of the groups of
protons within the molecule.
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