Please calculate theoretical grams of if 1.10 grams where collected in part 1 and 1.08 grams where collected part 2. Also calculate percent yeild. Reaction Conditions 1 1) In a 50-mL round-bottomed flask, with a spin bar, add 10mL of H2O solution which contains 1.0 mmol of 2-acetylpyridine. Stir the mixture vigorously. 2) Place 1.0 mmol of 4-nitrobenzaldehyde in a separate vial and dissolve using a minimum amount of warm MeOH. While still warm, add the solution of 4-nitrobenzaldehyde to the stirring mixture in the round-bottomed flask from step 1. 3) To this mixture add 0.25 mmol of Na2CO3 dissolved in 5 mL of H₂O. 4) After 1 hr of vigorous stirring, collect the solid product using vacuum filtration and wash with H2O (3 x 10mL) and a minimal amount of cold MeOH. 5) Allow the product to dry on the vacuum, determine the yield, melting point. Reaction Conditions 2 1) In a 50-mL round-bottomed flask, with a spin bar, add 10mL of H2O solution which contains 1.0 mmol of 2-acetylpyridine. Stir the mixture vigorously. 2) Place 1.0 mmol of 4-nitrobenzaldehyde in a separate vial and dissolve using a minimum amount of warm MeOH. While still warm, add the solution of 4-nitrobenzaldehyde to the stirring mixture in the round-bottomed flask. 3) To this mixture add 0.25 mmol of Na2CO3 dissolved in 5 mL of H₂O. 4) Attach a water-cooled reflux condenser and heat the reaction to reflux using an oil bath or a heating mantle. 5) After 1 hr of vigorous stirring at reflux, cool the reaction using an ice-water bath, collect the solid product using vacuum filtration. Wash the solid with H₂O (3 x 10mL) and a minimal amount of cold MeOH. 6) Allow the product to dry on the vacuum, determine the yield, melting point.
Please calculate theoretical grams of if 1.10 grams where collected in part 1 and 1.08 grams where collected part 2. Also calculate percent yeild. Reaction Conditions 1 1) In a 50-mL round-bottomed flask, with a spin bar, add 10mL of H2O solution which contains 1.0 mmol of 2-acetylpyridine. Stir the mixture vigorously. 2) Place 1.0 mmol of 4-nitrobenzaldehyde in a separate vial and dissolve using a minimum amount of warm MeOH. While still warm, add the solution of 4-nitrobenzaldehyde to the stirring mixture in the round-bottomed flask from step 1. 3) To this mixture add 0.25 mmol of Na2CO3 dissolved in 5 mL of H₂O. 4) After 1 hr of vigorous stirring, collect the solid product using vacuum filtration and wash with H2O (3 x 10mL) and a minimal amount of cold MeOH. 5) Allow the product to dry on the vacuum, determine the yield, melting point. Reaction Conditions 2 1) In a 50-mL round-bottomed flask, with a spin bar, add 10mL of H2O solution which contains 1.0 mmol of 2-acetylpyridine. Stir the mixture vigorously. 2) Place 1.0 mmol of 4-nitrobenzaldehyde in a separate vial and dissolve using a minimum amount of warm MeOH. While still warm, add the solution of 4-nitrobenzaldehyde to the stirring mixture in the round-bottomed flask. 3) To this mixture add 0.25 mmol of Na2CO3 dissolved in 5 mL of H₂O. 4) Attach a water-cooled reflux condenser and heat the reaction to reflux using an oil bath or a heating mantle. 5) After 1 hr of vigorous stirring at reflux, cool the reaction using an ice-water bath, collect the solid product using vacuum filtration. Wash the solid with H₂O (3 x 10mL) and a minimal amount of cold MeOH. 6) Allow the product to dry on the vacuum, determine the yield, melting point.
Chemistry
10th Edition
ISBN:9781305957404
Author:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Publisher:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Chapter1: Chemical Foundations
Section: Chapter Questions
Problem 1RQ: Define and explain the differences between the following terms. a. law and theory b. theory and...
Related questions
Question
None
Expert Solution
This question has been solved!
Explore an expertly crafted, step-by-step solution for a thorough understanding of key concepts.
Step by step
Solved in 2 steps with 1 images
Similar questions
Recommended textbooks for you
Chemistry
Chemistry
ISBN:
9781305957404
Author:
Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Publisher:
Cengage Learning
Chemistry
Chemistry
ISBN:
9781259911156
Author:
Raymond Chang Dr., Jason Overby Professor
Publisher:
McGraw-Hill Education
Principles of Instrumental Analysis
Chemistry
ISBN:
9781305577213
Author:
Douglas A. Skoog, F. James Holler, Stanley R. Crouch
Publisher:
Cengage Learning
Chemistry
Chemistry
ISBN:
9781305957404
Author:
Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Publisher:
Cengage Learning
Chemistry
Chemistry
ISBN:
9781259911156
Author:
Raymond Chang Dr., Jason Overby Professor
Publisher:
McGraw-Hill Education
Principles of Instrumental Analysis
Chemistry
ISBN:
9781305577213
Author:
Douglas A. Skoog, F. James Holler, Stanley R. Crouch
Publisher:
Cengage Learning
Organic Chemistry
Chemistry
ISBN:
9780078021558
Author:
Janice Gorzynski Smith Dr.
Publisher:
McGraw-Hill Education
Chemistry: Principles and Reactions
Chemistry
ISBN:
9781305079373
Author:
William L. Masterton, Cecile N. Hurley
Publisher:
Cengage Learning
Elementary Principles of Chemical Processes, Bind…
Chemistry
ISBN:
9781118431221
Author:
Richard M. Felder, Ronald W. Rousseau, Lisa G. Bullard
Publisher:
WILEY