PART B : ΑΝΙΟNΤΕSTS OPERATION OBSERVATION CONCLUSION Section 4: Test for Carbonate (CO,) ions 6 M HCI with Na,CO, Bubbling 6 M HCI with NaCl Clear solution 6 M HCI with Na,SO, Clear solution 6 M HCI with Na,PO. Clear solution 6 M HCI with unknown Clear solution

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PART B: AΝΙON TESTS
OPERATION
OBSERVATION
CONCLUSION
Section 4: Test for Carbonate (CO,*) ions
6 M HCI with Na,Co,
Bubbling
6 M HCI with NaCl
Clear solution
6 M HCI with Na.SO.
Clear solution
6 M HCI with Na,PO.
Clear solution
6 M HCI with unknown
Clear solution
Section 5: Test for Chloride (Cl) ions
After HNO, added
AGNO, with Na.CO, / HNO,
AGNO, with NaCl / HNO,
White precipitate
Clear solution
White precipitate
Precipitate stays
AGNO, with Na,SO,/ HNO,
Clear solution
Clear solution
AGNO, with Na,PO,/ HNO,
White precipitate
Clear solution
AGNO, with unknown / HNO, White precipitate
Clear solution
Section 6: Test for Sulfate (SO) ions
After HNO, added
BaCl: with Na.CO,/ HNO,
BaCl; with NaCl / HNO,
White precipitate
Clear solution
Clear solution
Clear solution
BaCl; with Na,SO,/ HNO,
White precipitate
Precipitate stays
BaCl; with Na,PO./ HNO,
White precipitate
Clear solution
BaCl, with unknown / HNO,
White precipitate
Precipitate stays
Section 7: Test for Phosphate (PO,") ions
(NH.).MoO, with Na.CO,
Clear solution
(NH,),MoO, with NaCI
Clear solution
(NH.),Mo0, with Na,SO,
Clear solution
(NH.),MoO, with Na,PO,
Yellow precipitate
(NH.).Mo0, with unknown
Clear solution
The unknown anion is
Summary from Observations and Conclusions in PARTS A and B:
30
Unknown Sample #
Cation
Anion
Unknown Name
Unknown Formula
Transcribed Image Text:PART B: AΝΙON TESTS OPERATION OBSERVATION CONCLUSION Section 4: Test for Carbonate (CO,*) ions 6 M HCI with Na,Co, Bubbling 6 M HCI with NaCl Clear solution 6 M HCI with Na.SO. Clear solution 6 M HCI with Na,PO. Clear solution 6 M HCI with unknown Clear solution Section 5: Test for Chloride (Cl) ions After HNO, added AGNO, with Na.CO, / HNO, AGNO, with NaCl / HNO, White precipitate Clear solution White precipitate Precipitate stays AGNO, with Na,SO,/ HNO, Clear solution Clear solution AGNO, with Na,PO,/ HNO, White precipitate Clear solution AGNO, with unknown / HNO, White precipitate Clear solution Section 6: Test for Sulfate (SO) ions After HNO, added BaCl: with Na.CO,/ HNO, BaCl; with NaCl / HNO, White precipitate Clear solution Clear solution Clear solution BaCl; with Na,SO,/ HNO, White precipitate Precipitate stays BaCl; with Na,PO./ HNO, White precipitate Clear solution BaCl, with unknown / HNO, White precipitate Precipitate stays Section 7: Test for Phosphate (PO,") ions (NH.).MoO, with Na.CO, Clear solution (NH,),MoO, with NaCI Clear solution (NH.),Mo0, with Na,SO, Clear solution (NH.),MoO, with Na,PO, Yellow precipitate (NH.).Mo0, with unknown Clear solution The unknown anion is Summary from Observations and Conclusions in PARTS A and B: 30 Unknown Sample # Cation Anion Unknown Name Unknown Formula
REPORT FORM
Experiment #9 – Analysis for Ions
Name
Section
Date
Unknown
Sample #
30
PART A: CATION TESTS
OPERATION
OBSERVATION
CONCLUSION
Section 1: Flame test for Na", K' and Ca ions
NaCl
Bright yellow
KCI
Lavender
CaCl,
Not very evident
Flame test for unknown Not very evident
Section 2: Test for Ca* ions
(NH.).C.O.with NaCl
Clear solution
(NH.).C.O.with KCI
Clear solution
(NH,),C,O, with CaCI,
White precipitate
(NH.).C.O.with FeCI,
Clear solution
(NH.).C.O, with unknown Clear solution
Section 2: Test for Fe* ions
KSCN with NaCl
Clear solution
KSCN with KCI
Clear solution
KSCN with CaCl,
Clear solution
KSCN with FeCl,
Blood red solution
KSCN with unknown
Blood red solution
The unknown cation is
Transcribed Image Text:REPORT FORM Experiment #9 – Analysis for Ions Name Section Date Unknown Sample # 30 PART A: CATION TESTS OPERATION OBSERVATION CONCLUSION Section 1: Flame test for Na", K' and Ca ions NaCl Bright yellow KCI Lavender CaCl, Not very evident Flame test for unknown Not very evident Section 2: Test for Ca* ions (NH.).C.O.with NaCl Clear solution (NH.).C.O.with KCI Clear solution (NH,),C,O, with CaCI, White precipitate (NH.).C.O.with FeCI, Clear solution (NH.).C.O, with unknown Clear solution Section 2: Test for Fe* ions KSCN with NaCl Clear solution KSCN with KCI Clear solution KSCN with CaCl, Clear solution KSCN with FeCl, Blood red solution KSCN with unknown Blood red solution The unknown cation is
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