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Question 2: Determine which unkown the following spectra depicts
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- Molecular Formula: C10H14 8 LOD TRANSMITTANCE1% D 4000 STRUCTURE: mult. t 2.72 q 6.90 S d t ppm 1.18 7.11 7.53 3000 H 6 4 1 2 1 5 2000 SPECTRUM 5 4 PPM HAVENUMBERI-L 1500 3 1000 5006. C8H100 11 TRANSMITTANCE LOD HSP-04-492 0+ 10 4000 9 3000 8 5 7 6 : 5 ppm 2000 4 HAVENUMBERI-l 2: 2 1 3 1500 2 سهر 1 1000 0 500 200 T 180 CDS-06-431 DEPT-90 T 160 DEPT-135 140 120 100 لك -2 peaks u ppm 80 60 40 20 0Transmittance (%) 100% 75% 50% 25% 0% 4000 3500 3000 OH 2500 2000 Spectrum 3B 1750 حسيمة 1500 Wavenumber (cm-¹) 1250 .OH 1000 OH 750 500
- QUESTION 5 The IR, 'H NMR and 1°C NMR spectra of compound P are shown below. The molecular formula for compound P is CsH;NO2. Identify three (3) important absorption peaks on the IR spectrum and indicate the bond and wavenumber associated with each peak. Elucidate the structure of compound P and assign each peak in the 'H and 13C NMR spectra. (Hint: The compound consists of more than one functional group). а. b.Lrdocaine USP (ATR) 95- 90 85 80 75 70 65 60 55 50 45 Lidocaine 40 4000 3500 3000 2500 2000 1500 1000 Wavenumbers (cm-1) %Transmittance IZ 3243.36 3021.30 2968.47 2921.13 2799.39 1661.66 1593.98 1491.43, 1449.061 422.12,384.681371.62 1291.03264.55 1206.99 1165.931119.56 1091.78072.77. 1034.33 970.79986.39 917.91, 885.23 763.76 703.94 615.01599.90Intensity (a.u.) 4000 3352 cm¹ 3500 3000 UNKNOWN B 1710 cm¹ 2000 1668 cm¹ 2500 Wavenumber (cm¹¹) 1500 1101 cm 1000 500
- Spectrum 28 100% 75%- 50%- 25% 0% 3500 2500 1750 1250 750 4000 3000 2000 1500 1000 50 Wavenumber (cm) NH2 Transmittance (%)100 - 80 60 40 20 10 15 20 25 30 35 40 45 50 55 60 m/z Absorbance / % 50- 100+ 4000 3000 2500 2000 1500 1000 500 Wavenumbers / cm Relative Intensity / %MASS % of Base Peak IR 100 5045 % Transmittance 100 T 50 4000 1540 ¹H NMR 300 MHz t 557 5.0 Hz 60 alla illle 677 69 1140 4.5 70 4.0 13C/DEPT NMR 75.5 MHz 3000 130 120 110 100 الد الله da 110 113 100 110 mm 817 Hz 500 90 80 m/z Wavenumber (cm-¹) 3.5 ми линия 80 90 480 Hz 957 3.0 70 2000 440 2.5 Hz 1450 2.0 -1126 120 1000 60 50 40 30 1287 130 1.5 ppm 20 ppm
- Following are infrared spectra of 2-methyl-1-butanol and tert-butyl methyl ether. Assign each compound its correct spectrum. Micrometers 2.5 100 3. 4. 9. 13 8 10 11 12 14 15 20 90 80 70 50 40 30 20 10 4000 3600 3200 2800 2400 2000 1800 1600 1400 1200 1000 800 600 400 Wavenumber (cm-1) Transmittance (%)You will check the outcome of reaction via infra-red spectroscopy: what are the diagnostic functional group peaks for the following compounds? You should also indicate the stretching motions responsible for absorbance. Dilantin benzil (unreacted starting material) Urea (unreacted starting material)Below are the IR and mass spectra of an unknown compound. % Transmittance Relative Intensity 100 80- 60 40 20 0 4000 100 80 60 40 20 10 3500 3000 2500 2000 1500 Wavenumber (cm-1) elle 20 30 40 50 60 m/z 70 mm 1000 500 80 90 100