Nitrous Acid Test Procedure: Make a solution of 4 grams NaNO3 in 16 mL water. Put 2 mL of concentrated hydrochloric acid into a 10x75-mm test tube and add 0.5 ml of amine. Cool the solution in a water-ice slush to zero degrees celcius. Add the nitrile solution slowly, dropwise, until a drop of the reaction mixture gives a blue spot on starch-iodide paper. The following should be tested: (NOTE: Include the observations and reaction equation) A. PRIMARY ALIPHATIC AMINES (Like Butylamine of Cyclohexylamine) B. PRIMARY AROMATIC AMINES I. Aniline + nitrous acid; then heat. II. Aniline + nitrous acid; then B-Napthol.
Nitrous Acid Test Procedure: Make a solution of 4 grams NaNO3 in 16 mL water. Put 2 mL of concentrated hydrochloric acid into a 10x75-mm test tube and add 0.5 ml of amine. Cool the solution in a water-ice slush to zero degrees celcius. Add the nitrile solution slowly, dropwise, until a drop of the reaction mixture gives a blue spot on starch-iodide paper. The following should be tested: (NOTE: Include the observations and reaction equation) A. PRIMARY ALIPHATIC AMINES (Like Butylamine of Cyclohexylamine) B. PRIMARY AROMATIC AMINES I. Aniline + nitrous acid; then heat. II. Aniline + nitrous acid; then B-Napthol.
Chemistry
10th Edition
ISBN:9781305957404
Author:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Publisher:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Chapter1: Chemical Foundations
Section: Chapter Questions
Problem 1RQ: Define and explain the differences between the following terms. a. law and theory b. theory and...
Related questions
Question
Nitrous Acid Test
Procedure: Make a solution of 4 grams NaNO3 in 16 mL water. Put 2 mL of concentrated hydrochloric acid into a 10x75-mm test tube and add 0.5 ml of amine. Cool the solution in a water-ice slush to zero degrees celcius. Add the nitrile solution slowly, dropwise, until a drop of the reaction mixture gives a blue spot on starch-iodide paper.
The following should be tested: (NOTE: Include the observations and reaction equation)
A. PRIMARY ALIPHATIC
B. PRIMARY
I. Aniline + nitrous acid; then heat.
II. Aniline + nitrous acid; then B-Napthol.
Expert Solution
This question has been solved!
Explore an expertly crafted, step-by-step solution for a thorough understanding of key concepts.
This is a popular solution!
Trending now
This is a popular solution!
Step by step
Solved in 2 steps with 3 images
Knowledge Booster
Learn more about
Need a deep-dive on the concept behind this application? Look no further. Learn more about this topic, chemistry and related others by exploring similar questions and additional content below.Recommended textbooks for you
Chemistry
Chemistry
ISBN:
9781305957404
Author:
Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Publisher:
Cengage Learning
Chemistry
Chemistry
ISBN:
9781259911156
Author:
Raymond Chang Dr., Jason Overby Professor
Publisher:
McGraw-Hill Education
Principles of Instrumental Analysis
Chemistry
ISBN:
9781305577213
Author:
Douglas A. Skoog, F. James Holler, Stanley R. Crouch
Publisher:
Cengage Learning
Chemistry
Chemistry
ISBN:
9781305957404
Author:
Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Publisher:
Cengage Learning
Chemistry
Chemistry
ISBN:
9781259911156
Author:
Raymond Chang Dr., Jason Overby Professor
Publisher:
McGraw-Hill Education
Principles of Instrumental Analysis
Chemistry
ISBN:
9781305577213
Author:
Douglas A. Skoog, F. James Holler, Stanley R. Crouch
Publisher:
Cengage Learning
Organic Chemistry
Chemistry
ISBN:
9780078021558
Author:
Janice Gorzynski Smith Dr.
Publisher:
McGraw-Hill Education
Chemistry: Principles and Reactions
Chemistry
ISBN:
9781305079373
Author:
William L. Masterton, Cecile N. Hurley
Publisher:
Cengage Learning
Elementary Principles of Chemical Processes, Bind…
Chemistry
ISBN:
9781118431221
Author:
Richard M. Felder, Ronald W. Rousseau, Lisa G. Bullard
Publisher:
WILEY