In this part we will provide conclusive proof of the stereochemistry of the product by preparing the acetonide of hydrobenzoin and examining its 'H NMR spectrum. An acetonide is a cyclic ketal prepared from acetone and either a 1,2- or a 1,3-diol. Our procedure uses anhydrous ferric chloride as a Lewis acid catalyst for the preparation of the acetonide. OH OH Hydrobenzoin Experimental Procedure H3C1 CH3 FeCl3 CH3 gx CH3
In this part we will provide conclusive proof of the stereochemistry of the product by preparing the acetonide of hydrobenzoin and examining its 'H NMR spectrum. An acetonide is a cyclic ketal prepared from acetone and either a 1,2- or a 1,3-diol. Our procedure uses anhydrous ferric chloride as a Lewis acid catalyst for the preparation of the acetonide. OH OH Hydrobenzoin Experimental Procedure H3C1 CH3 FeCl3 CH3 gx CH3
Chemistry
10th Edition
ISBN:9781305957404
Author:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Publisher:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Chapter1: Chemical Foundations
Section: Chapter Questions
Problem 1RQ: Define and explain the differences between the following terms. a. law and theory b. theory and...
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Transcribed Image Text:In this part we will provide conclusive proof of the stereochemistry of the product by preparing the
acetonide of hydrobenzoin and examining its 'H NMR spectrum. An acetonide is a cyclic ketal prepared
from acetone and either a 1,2- or a 1,3-diol. Our procedure uses anhydrous ferric chloride as a Lewis acid
catalyst for the preparation of the acetonide.
OH
OH
Hydrobenzoin
Experimental Procedure
H3C1 CH3
FeCl3
CH3
gx
CH3
Note: For the acetonide preparation to be successful, it is essential that all reagents and
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