The purpose of this experiment is to use both extraction and crystallization techniques to separate a solid mixture of organic compounds. You will receive a packet with 1 g of a unknown (pH is basic) amide solid sample which will contain three components, one from each group:Group 1 (~50% wt): ethyl 4-aminobenzoate, ortho-toluic acid, or benzoic acid Group 2 (~40% wt): fluorene, 1,4-dibromobenzene, benzil, benzoinGroup 3 (~10% wt): fluorene, 1,4-dibromobenzene, benzil, benzoin (but not the same as Group 2 compound)Create a lab procedure that will allow you to successfully isolate, purify, and identify the two major (Group 1 and Group 2) components of the unknown amide sample. reagents that can be used are 1M HCl, 6M HCl, 1M NaOH, 6M NaOH, diethyl ether, and methylene chloride

Lab procedure – The laboratory procedure involves isolating, purifying, and identifying Group 1 and…

Answered: extraction and crystallization…

Chemistry

10th Edition

ISBN:9781305957404

Author:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste

Publisher:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste

Chapter1: Chemical Foundations

Section: Chapter Questions

Problem 1RQ: Define and explain the differences between the following terms. a. law and theory b. theory and...

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The purpose of this experiment is to use both extraction and crystallization techniques to separate a solid mixture of organic compounds. You will receive a packet with 1 g of a unknown (pH is basic) amide solid sample which will contain three components, one from each group:

Group 1 (~50% wt): ethyl 4-aminobenzoate, ortho-toluic acid, or benzoic acid
Group 2 (~40% wt): fluorene, 1,4-dibromobenzene, benzil, benzoin
Group 3 (~10% wt): fluorene, 1,4-dibromobenzene, benzil, benzoin (but not the same as Group 2 compound)

Create a lab procedure that will allow you to successfully isolate, purify, and identify the two major (Group 1 and Group 2) components of the unknown amide sample.

reagents that can be used are 1M HCl, 6M HCl, 1M NaOH, 6M NaOH, diethyl ether, and methylene chloride

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