Chemistry
10th Edition
ISBN:9781305957404
Author:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Publisher:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Chapter1: Chemical Foundations
Section: Chapter Questions
Problem 1RQ: Define and explain the differences between the following terms. a. law and theory b. theory and...
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![### Experiment 6: IR Spectroscopy
#### Reaction Schemes and Descriptions
**1. Conversion of Cyclohexanol to Cyclohexanone**
- **Reactants:** Cyclohexanol
- **Reagents:** NaOCl, AcOH, 45-50°C
- **Product:** Cyclohexanone
**Chemical Reaction:**
\[ \text{Cyclohexanol} \xrightarrow{\text{NaOCl, AcOH, 45-50°C}} \text{Cyclohexanone} \]
**2. Oxidation of Steroid Alcohol to Steroid Ketone**
- **Reactants:** Steroid Alcohol
- **Reagents:** MCPBA in CH₂Cl₂
- **Product:** Steroid Ketone
**Chemical Reaction:**
\[ \text{Steroid Alcohol} \xrightarrow{\text{MCPBA, CH₂Cl₂}} \text{Steroid Ketone} \]
**3. Formation of Phenyl Ether**
- **Reactants:** Chlorobenzene and Phenol
- **Reagents:** K₂CO₃
- **Product:** Phenyl Ether
**Chemical Reaction:**
\[ \text{Chlorobenzene} + \text{Phenol} \xrightarrow{\text{K₂CO₃}} \text{Phenyl Ether} \]
**4. Synthesis of Benzoic Acid via Grignard Reaction**
- **Reactants:** Bromobenzene
- **Reagents:**
1. Mg
2. CO₂
- **Product:** Benzoic Acid
**Chemical Reaction:**
\[ \text{Bromobenzene} \xrightarrow{\text{1. Mg, 2. CO₂}} \text{Benzoic Acid} \]
**5. Reduction of Benzylideneacetophenone to 1,2-Diphenylethane-1,2-diol**
- **Reactants:** Benzylideneacetophenone
- **Reagents:** NaBH₄, EtOH
- **Product:** 1,2-Diphenylethane-1,2-diol
**Chemical Reaction:**
\[ \text{Benzylideneacetophenone} \xrightarrow{\text{NaBH₄, EtOH}} \text{1,2-Diphenylethane-1,](/v2/_next/image?url=https%3A%2F%2Fcontent.bartleby.com%2Fqna-images%2Fquestion%2F3626a8b8-545e-40de-96fe-d72df53f2c0e%2F9258c3d2-afac-4849-b5d7-2ebf27f15a39%2Feofiz6u_processed.jpeg&w=3840&q=75)
Transcribed Image Text:### Experiment 6: IR Spectroscopy
#### Reaction Schemes and Descriptions
**1. Conversion of Cyclohexanol to Cyclohexanone**
- **Reactants:** Cyclohexanol
- **Reagents:** NaOCl, AcOH, 45-50°C
- **Product:** Cyclohexanone
**Chemical Reaction:**
\[ \text{Cyclohexanol} \xrightarrow{\text{NaOCl, AcOH, 45-50°C}} \text{Cyclohexanone} \]
**2. Oxidation of Steroid Alcohol to Steroid Ketone**
- **Reactants:** Steroid Alcohol
- **Reagents:** MCPBA in CH₂Cl₂
- **Product:** Steroid Ketone
**Chemical Reaction:**
\[ \text{Steroid Alcohol} \xrightarrow{\text{MCPBA, CH₂Cl₂}} \text{Steroid Ketone} \]
**3. Formation of Phenyl Ether**
- **Reactants:** Chlorobenzene and Phenol
- **Reagents:** K₂CO₃
- **Product:** Phenyl Ether
**Chemical Reaction:**
\[ \text{Chlorobenzene} + \text{Phenol} \xrightarrow{\text{K₂CO₃}} \text{Phenyl Ether} \]
**4. Synthesis of Benzoic Acid via Grignard Reaction**
- **Reactants:** Bromobenzene
- **Reagents:**
1. Mg
2. CO₂
- **Product:** Benzoic Acid
**Chemical Reaction:**
\[ \text{Bromobenzene} \xrightarrow{\text{1. Mg, 2. CO₂}} \text{Benzoic Acid} \]
**5. Reduction of Benzylideneacetophenone to 1,2-Diphenylethane-1,2-diol**
- **Reactants:** Benzylideneacetophenone
- **Reagents:** NaBH₄, EtOH
- **Product:** 1,2-Diphenylethane-1,2-diol
**Chemical Reaction:**
\[ \text{Benzylideneacetophenone} \xrightarrow{\text{NaBH₄, EtOH}} \text{1,2-Diphenylethane-1,
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